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Solid-state NMR: Methods for biological solids
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
Solid-state NMR spectroscopy
Solid-state nuclear magnetic resonance (NMR) spectroscopy is an atomic-level method to
determine the chemical structure, 3D structure and dynamics of solids and semi-solids. This …
determine the chemical structure, 3D structure and dynamics of solids and semi-solids. This …
Structure and drug binding of the SARS-CoV-2 envelope protein transmembrane domain in lipid bilayers
An essential protein of the SARS-CoV-2 virus, the envelope protein E, forms a
homopentameric cation channel that is important for virus pathogenicity. Here we report a …
homopentameric cation channel that is important for virus pathogenicity. Here we report a …
The ladder of life detection
We describe the history and features of the Ladder of Life Detection, a tool intended to guide
the design of investigations to detect microbial life within the practical constraints of robotic …
the design of investigations to detect microbial life within the practical constraints of robotic …
Rapid proton-detected NMR assignment for proteins with fast magic angle spinning
E Barbet-Massin, AJ Pell, JS Retel… - Journal of the …, 2014 - ACS Publications
Using a set of six 1H-detected triple-resonance NMR experiments, we establish a method for
sequence-specific backbone resonance assignment of magic angle spinning (MAS) nuclear …
sequence-specific backbone resonance assignment of magic angle spinning (MAS) nuclear …
Solid‐state NMR spectroscopic methods in chemistry
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …
analysis, structure determination, and the study of dynamics in organic, inorganic, and …
3D TEDOR NMR Experiments for the Simultaneous Measurement of Multiple Carbon−Nitrogen Distances in Uniformly 13C,15N-Labeled Solids
We describe three-dimensional magic-angle-spinning NMR experiments for the
simultaneous measurement of multiple carbon− nitrogen distances in uniformly 13C, 15N …
simultaneous measurement of multiple carbon− nitrogen distances in uniformly 13C, 15N …
Dynamic nuclear polarization with a rigid biradical
A new polarizing agent with superior performance in dynamic nuclear polarization
experiments is introduced, and utilizes two TEMPO (2, 2, 6, 6‐tetramethylpiperidine‐1‐oxyl) …
experiments is introduced, and utilizes two TEMPO (2, 2, 6, 6‐tetramethylpiperidine‐1‐oxyl) …
Dynamic nuclear polarization at 9 T using a novel 250 GHz gyrotron microwave source
In this communication, we report enhancements of nuclear spin polarization by dynamic
nuclear polarization (DNP) in static and spinning solids at a magnetic field strength of 9T …
nuclear polarization (DNP) in static and spinning solids at a magnetic field strength of 9T …
Broadband homonuclear correlation spectroscopy driven by combined R2nv sequences under fast magic angle spinning for NMR structural analysis of organic and …
We recently described a family of experiments for R2nv Driven Spin Diffusion (RDSD)
spectroscopy suitable for homonuclear correlation experiments under fast MAS conditions …
spectroscopy suitable for homonuclear correlation experiments under fast MAS conditions …