This overview highlights the emergent area of mechanochemical reactions for making active
pharmaceutical ingredients (APIs), and covers the latest advances in the recently …

π–π stacking interactions, as a kind of attractive and nondestructive noncovalent interaction,
have been widely explored for the applications in modern chemistry, molecular biology, and …

We present a solvent-free, green, and rapid mechanochemical route for the synthesis of a
series of zirconium metal–organic frameworks (MOFs) composed of Zr6 cluster nodes, UiO …

Mechanistic understanding of mechanochemical reactions is sparse and has been acquired
mostly by stepwise ex situ analysis. We describe herein an unprecedented laboratory …

We provide a brief overview of the first techniques for direct, real-time observation of
mechanochemical reactions by milling. Whereas mechanisms and kinetics of solid-state …

Mechanosynthesis has attracted the attention of chemists and materials scientists [1]
interested in new synthetic opportunities offered by a fully or nearly solvent-free reaction …

We describe the only currently available protocol for in situ, real-time monitoring of
mechanochemical reactions and intermediates by X-ray powder diffraction. Although …

We have applied in situ monitoring of mechanochemical reactions by high-energy
synchrotron powder X-ray diffraction to study the role of liquid additives on the …

We describe the first in situ and real-time study of a mechanochemical reaction by variable-
temperature synchrotron powder X-ray diffraction. Using the dry milling synthesis of a …

Mechanochemical reactions by ball milling are becoming increasingly popular across a
wide range of chemical sciences, but understanding and evaluation of temperature during …