Meeting the UN sustainable development goals with mechanochemistry

J Alić, MC Schlegel, F Emmerling… - Angewandte Chemie …, 2024 - Wiley Online Library
Chemistry traditionally relies on reactions in solution, but this method is increasingly
problematic due to the scale of chemical processes and their economic and environmental …

Opportunities and Challenges in Applying Solid‐State NMR Spectroscopy in Organic Mechanochemistry

IAA Silva, E Bartalucci, C Bolm… - Advanced Materials, 2023 - Wiley Online Library
In recent years it is shown that mechanochemical strategies can be beneficial in directed
conversions of organic compounds. Finding new reactions proved difficult, and due to the …

NMR in operando monitoring of mechanochemically accelerated sublimations

F Puccetti, T Rinesch, S Suljić, K Rahimi, A Herrmann… - Chem, 2023 - cell.com
Solid-solid interactions in optically active materials lead to the phenomena of spontaneous
enantioenrichment, with implications in prebiotic chemistry and materials purification …

From Inert to Catalytically Active Milling Media: Galvanostatic Coating for Direct Mechanocatalysis

M Wohlgemuth, M Mayer, M Rappen… - Angewandte Chemie …, 2022 - Wiley Online Library
The inert milling balls, commonly utilized in mechanochemical reactions, were coated with a
layer of Pd and utilized as catalyst in the direct mechanocatalytic Suzuki reaction. With high …

Intermediates in Mechanochemical Reactions

KJ Ardila‐Fierro, JG Hernández - … Chemie International Edition, 2024 - Wiley Online Library
Mechanochemical reactions offer methodological and environmental advantages for
chemical synthesis, constantly attracting attention within the scientific community. Besides …

Mechanosynthesis of sulfonamides via a telescopic, environmentally friendly, and cost-effective process

F Cuccu, A Porcheddu - Green Chemistry, 2024 - pubs.rsc.org
Herein, we demonstrate a solvent-free mechanochemical approach involving a one-pot-
double-step procedure mediated by solid sodium hypochlorite (NaOCl· 5H2O) for the …

Mechanochemical Fischer indolisation: an eco-friendly design for a timeless reaction

A Porcheddu, R Mocci, M Brindisi, F Cuccu… - Green …, 2022 - pubs.rsc.org
We developed an environmentally friendly mechanochemical protocol to induce an effective
Fischer indolisation to synthesize indoles and indolines taking advantage of oxalic acid and …

SpeedMixing: Rapid tribochemical synthesis and discovery of pharmaceutical cocrystals without milling or grinding media

Y Teoh, G Ayoub, I Huskić, HM Titi… - Angewandte Chemie …, 2022 - Wiley Online Library
We present SpeedMixing, a rapid blending technology, as an approach for fast
mechanosynthesis and discovery of model pharmaceutical cocrystals through rapid …

Critical review on mechanochemical fabrication of full-carbon graphyne material

L Wang, Z Hao, S Chen, H Chen, Y Lou, C He… - Progress in Materials …, 2024 - Elsevier
Graphyne, a novel regularly sp-/sp 2-hybridized carbon allotrope, has attracted significant
interest in synthetic chemistry and various applications. As a promising approach for …

Phenytoin-associated movement disorder: A literature review

JP Rissardo, ALF Caprara - Tzu chi medical journal, 2022 - journals.lww.com
Phenytoin (PHT) was first synthesized as a barbiturate derivative and was approved in 1953
by the Food and Drug Administration. This work aimed to review the pathophysiology …