Mechanochemistry: opportunities for new and cleaner synthesis

SL James, CJ Adams, C Bolm, D Braga… - Chemical Society …, 2012 - pubs.rsc.org
The aim of this critical review is to provide a broad but digestible overview of
mechanochemical synthesis, ie reactions conducted by grinding solid reactants together …

Eco-friendly physical activation methods for Suzuki–Miyaura reactions

K Martina, M Manzoli, E Calcio Gaudino, G Cravotto - Catalysts, 2017 - mdpi.com
Eco-compatible activation methods in Suzuki–Miyaura cross-coupling reactions offer
challenging opportunities for the design of clean and efficient synthetic processes. The main …

An efficient green synthesis of 2-arylbenzothiazole analogues as potent antibacterial and anticancer agents

M Chhabra, S Sinha, S Banerjee, P Paira - Bioorganic & medicinal …, 2016 - Elsevier
We have demonstrated a novel and green approach for the synthesis of 2-substituted
benzothiazole analogues. A number of 2-aryl and heteroaryl benzothiazole scaffolds were …

Microwave-assisted and efficient solvent-free knoevenagel condensation. A sustainable protocol using porous calcium hydroxyapatite as catalyst

S Mallouk, K Bougrin, A Laghzizil, R Benhida - Molecules, 2010 - mdpi.com
A sustainable Knoevenagel condensation of a series of aldehydes with malononitrile and
ethyl cyanoacetate is described. The process is based on the combination of microwave …

Solvent-free aryl amination catalysed by [Pd (NHC)] complexes

A Chartoire, A Boreux, AR Martin, SP Nolan - RSC Advances, 2013 - pubs.rsc.org
A highly effective solvent-free protocol for the Buchwald–Hartwig amination of unactivated
aryl chlorides is described. The effect of various [Pd (NHC)] pre-catalyst systems on the …

Palladium on carbon-catalyzed solvent-free and solid-phase hydrogenation and Suzuki–Miyaura reaction

Y Monguchi, Y Fujita, S Hashimoto, M Ina, T Takahashi… - Tetrahedron, 2011 - Elsevier
The solvent-free and solid-phase hydrogenation of various reducible functionalities was
efficiently catalyzed by heterogeneous palladium on carbon (Pd/C) under ambient hydrogen …

Pseudo‐Solid‐State Suzuki–Miyaura Reaction and the Role of Water Formed by Dehydration of Arylboronic Acids

EO Pentsak, VP Ananikov - European Journal of Organic …, 2019 - Wiley Online Library
Solvent‐free reactions belong to a very attractive area of organic chemistry. The solvent‐free
Suzuki–Miyaura coupling is of special importance due to the problem of catalyst leaching in …

Cu (ii), Ir (i) and CuO nanocatalyzed mild synthesis of luminescent symmetrical and unsymmetrical bis (triazolylmethyl) quinoxalines: biocompatibility, cytotoxicity, live …

S Maiti, N Roy, LT Babu, P Moharana… - New Journal of …, 2020 - pubs.rsc.org
Quinoxaline derivatives play versatile roles in various fields of science. Thus different types
of scaffolds have been designed with these quinoxaline moieties to make them more …

Phosphatase CDC25B inhibitors produced by basic alumina-supported one-pot gram-scale synthesis of fluorinated 2-alkylthio-4-aminoquinazolines using microwave …

J Liu, YL Wang, JH Zhang, JS Yang, HC Mou, J Lin… - ACS …, 2018 - ACS Publications
An efficient, environmentally benign, and inexpensive procedure has been developed for
the synthesis of fluorinated 2-alkylthio-4-aminoquinazolines by microwave irradiation using …

Suzuki-miyaura cross-coupling reaction catalyzed by supported palladium under microwave irradiation

Q Han Li, Y Ding, G Zhang, Z Zhang… - Current Organic …, 2017 - benthamdirect.com
Organic synthesis efficiency can take considerable advantage from microwave heating.
Compared to conventional heating, it allows to improve the reactions speed and yield …