Spin hyperpolarization in modern magnetic resonance

J Eills, D Budker, S Cavagnero, EY Chekmenev… - Chemical …, 2023 - ACS Publications
Magnetic resonance techniques are successfully utilized in a broad range of scientific
disciplines and in various practical applications, with medical magnetic resonance imaging …

Solid-state NMR investigations of extracellular matrixes and cell walls of algae, bacteria, fungi, and plants

N Ghassemi, A Poulhazan, F Deligey… - Chemical …, 2021 - ACS Publications
Extracellular matrixes (ECMs), such as the cell walls and biofilms, are important for
supporting cell integrity and function and regulating intercellular communication. These …

Dynamic nuclear polarization for sensitivity enhancement in biomolecular solid-state NMR

T Biedenbänder, V Aladin, S Saeidpour… - Chemical …, 2022 - ACS Publications
Solid-state NMR with magic-angle spinning (MAS) is an important method in structural
biology. While NMR can provide invaluable information about local geometry on an atomic …

Biomolecular and biological applications of solid-state NMR with dynamic nuclear polarization enhancement

WY Chow, G De Paëpe, S Hediger - Chemical Reviews, 2022 - ACS Publications
Solid-state NMR spectroscopy (ssNMR) with magic-angle spinning (MAS) enables the
investigation of biological systems within their native context, such as lipid membranes, viral …

Recent developments in MAS DNP-NMR of materials

AGM Rankin, J Trébosc, F Pourpoint… - Solid State Nuclear …, 2019 - Elsevier
Solid-state NMR spectroscopy is a powerful technique for the characterization of the atomic-
level structure and dynamics of materials. Nevertheless, the use of this technique is often …

Dynamic nuclear polarization enhancement of 200 at 21.15 T enabled by 65 kHz magic angle spinning

P Berruyer, S Björgvinsdóttir… - The journal of …, 2020 - ACS Publications
Solid-state nuclear magnetic resonance under magic angle spinning (MAS) enhanced with
dynamic nuclear polarization (DNP) is a powerful approach to characterize many important …

Highly efficient polarizing agents for MAS‐DNP of proton‐dense molecular solids

R Harrabi, T Halbritter, F Aussenac… - Angewandte …, 2022 - Wiley Online Library
Efficiently hyperpolarizing proton‐dense molecular solids through dynamic nuclear
polarization (DNP) solid‐state NMR is still an unmet challenge. Polarizing agents (PAs) …

TinyPols: a family of water-soluble binitroxides tailored for dynamic nuclear polarization enhanced NMR spectroscopy at 18.8 and 21.1 T

A Lund, G Casano, G Menzildjian, M Kaushik… - Chemical …, 2020 - pubs.rsc.org
Dynamic Nuclear Polarization (DNP) has recently emerged as a key method to increase the
sensitivity of solid-state NMR spectroscopy under Magic Angle Spinning (MAS). While …

High-field pulsed EPR spectroscopy under magic angle spinning

O Nir-Arad, AB Fialkov, DH Shlomi, N Manukovsky… - Science …, 2024 - science.org
In this work, we demonstrate the first pulsed electron paramagnetic resonance (EPR)
experiments performed under magic angle spinning (MAS) at high magnetic field. Unlike …

Solid-state NMR of plant and fungal cell walls: a critical review

W Zhao, LD Fernando, A Kirui, F Deligey… - Solid state nuclear …, 2020 - Elsevier
The cell walls of plants and microbes are a central source for bio-renewable energy and the
major targets of antibiotics and antifungal agents. It is highly challenging to determine the …