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Quantitative scanning transmission electron microscopy for materials science: Imaging, diffraction, spectroscopy, and tomography
C Ophus - Annual Review of Materials Research, 2023 - annualreviews.org
Scanning transmission electron microscopy (STEM) is one of the most powerful
characterization tools in materials science research. Due to instrumentation developments …
characterization tools in materials science research. Due to instrumentation developments …
The role of high-resolution transmission electron microscopy and aberration corrected scanning transmission electron microscopy in unraveling the structure-property …
Platinum-based fuel cell electrocatalysts are structured on a nano level in order to extend
their active surface area and maximize the utilization of precious and scarce platinum. Their …
their active surface area and maximize the utilization of precious and scarce platinum. Their …
Grain boundary engineering for efficient and durable electrocatalysis
X Geng, M Vega-Paredes, Z Wang, C Ophus… - Nature …, 2024 - nature.com
Grain boundaries in noble metal catalysts have been identified as critical sites for enhancing
catalytic activity in electrochemical reactions such as the oxygen reduction reaction …
catalytic activity in electrochemical reactions such as the oxygen reduction reaction …
Diameter-dependent phase selectivity in 1D-confined tungsten phosphides
Topological materials confined in 1D can transform computing technologies, such as 1D
topological semimetals for nanoscale interconnects and 1D topological superconductors for …
topological semimetals for nanoscale interconnects and 1D topological superconductors for …
Unsupervised machine learning and cepstral analysis with 4D-STEM for characterizing complex microstructures of metallic alloys
Four-dimensional scanning transmission electron microscopy, coupled with a wide array of
data analytics, has unveiled new insights into complex materials. Here, we introduce a …
data analytics, has unveiled new insights into complex materials. Here, we introduce a …
Direct Measurement of the Thermal Expansion Coefficient of Epitaxial WSe2 by Four-Dimensional Scanning Transmission Electron Microscopy
Current reports of thermal expansion coefficients (TEC) of two-dimensional (2D) materials
show large discrepancies that span orders of magnitude. Determining the TEC of any 2D …
show large discrepancies that span orders of magnitude. Determining the TEC of any 2D …
Disentangling multiple scattering with deep learning: application to strain map** from electron diffraction patterns
A fast, robust pipeline for strain map** of crystalline materials is important for many
technological applications. Scanning electron nanodiffraction allows us to calculate strain …
technological applications. Scanning electron nanodiffraction allows us to calculate strain …
From STEM to 4D STEM: Ultrafast diffraction map** with a hybrid-pixel detector
DG Stroppa, M Meffert, C Hoermann… - Microscopy …, 2023 - academic.oup.com
Abstract 4D scanning transmission electron microscope (STEM) techniques have been
increasingly featured among the electron microscopy characterization approaches, as they …
increasingly featured among the electron microscopy characterization approaches, as they …
Cryogenic 4D-STEM analysis of an amorphous-crystalline polymer blend: Combined nanocrystalline and amorphous phase map**
Understanding and visualizing the heterogeneous structure of immiscible semicrystalline
polymer systems is critical for optimizing their morphology and microstructure. We …
polymer systems is critical for optimizing their morphology and microstructure. We …
Multimodal characterization of crystal structure and formation in rubrene thin films reveals erasure of orientational discontinuities
Multimodal multiscale characterization provide opportunities to study organic
semiconducting thin films with multiple length scales, across multiple platforms, to elucidate …
semiconducting thin films with multiple length scales, across multiple platforms, to elucidate …