Toward autonomous laboratories: Convergence of artificial intelligence and experimental automation

Y **e, K Sattari, C Zhang, J Lin - Progress in Materials Science, 2023‏ - Elsevier
The ever-increasing demand for novel materials with superior properties inspires retrofitting
traditional research paradigms in the era of artificial intelligence and automation. An …

Process analytical technologies and self-optimization algorithms in automated pharmaceutical continuous manufacturing

P Liu, H **, Y Chen, D Wang, H Yan, M Wu… - Chinese Chemical …, 2024‏ - Elsevier
The pharmaceutical industry is now paying increased attention to continuous manufacturing.
While the revolution to continuous and automated manufacturing is deepening in most of the …

Review of low-cost self-driving laboratories in chemistry and materials science: the “frugal twin” concept

S Lo, SG Baird, J Schrier, B Blaiszik, N Carson… - Digital …, 2024‏ - pubs.rsc.org
This review proposes the concept of a “frugal twin,” similar to a digital twin, but for physical
experiments. Frugal twins range from simple toy examples to low-cost surrogates of high …

Autonomous execution of highly reactive chemical transformations in the Schlenkputer

NL Bell, F Boser, A Bubliauskas, DR Willcox… - Nature Chemical …, 2024‏ - nature.com
We design a modular programmable inert-atmosphere Schlenkputer (Schlenk-line
computer) for the synthesis and manipulation of highly reactive compounds, including those …

Multistep automated synthesis of pharmaceuticals

G Wang, HT Ang, SR Dubbaka, P O'Neill, J Wu - Trends in Chemistry, 2023‏ - cell.com
Multistep automated pharmaceutical syntheses have been a long-term industrial goal.
Automation not only enables the rapid and highly efficient preparation of organic …

An Adaptive Auto‐Synthesizer Using Online PAT Feedback to Flexibly Perform a Multistep Reaction

J Liu, Y Sato, F Yang, AJ Kukor, JE Hein - Chemistry‐Methods, 2022‏ - Wiley Online Library
Automated chemical synthesizers have become more common in recent years but struggle
to apply rigid procedures to broad substrate scopes. We have developed an adaptive auto …

Robotic modules for the programmable chemputation of molecules and materials

D Salley, JS Manzano, PJ Kitson, L Cronin - ACS Central Science, 2023‏ - ACS Publications
Before leveraging big data methods like machine learning and artificial intelligence (AI) in
chemistry, there is an imperative need for an affordable, universal digitization standard. This …

Reaction Kinetics using a Chemputable Framework for Data Collection and Analysis

BM Matysiak, D Thomas, L Cronin - Angewandte Chemie, 2024‏ - Wiley Online Library
Automated chemistry platforms have been widely explored, but many focus on fixed tasks for
chemical synthesis or analysis. However, a typical synthetic chemistry workflow utilizes both …

Autonomous experimental systems in materials science

N Ishizuki, R Shimizu, T Hitosugi - Science and Technology of …, 2023‏ - Taylor & Francis
The emergence of autonomous experimental systems integrating machine learning and
robots is ushering in a paradigm shift in materials science. Using computer algorithms and …

Automated library generation and serendipity quantification enables diverse discovery in coordination chemistry

DJ Kowalski, CM MacGregor, DL Long… - Journal of the …, 2023‏ - ACS Publications
Library generation experiments are a key part of the discovery of new materials, methods,
and models in chemistry, but the question of how to generate high quality libraries to enable …