Structural characterization of biomaterials by means of small angle X-rays and neutron scattering (SAXS and SANS), and light scattering experiments

D Lombardo, P Calandra, MA Kiselev - Molecules, 2020 - mdpi.com
Scattering techniques represent non-invasive experimental approaches and powerful tools
for the investigation of structure and conformation of biomaterial systems in a wide range of …

Unified mechanistic interpretation of amine-assisted silica synthesis methods to enable design of more complex materials

JRH Manning, C Brambila… - Molecular Systems Design …, 2021 - pubs.rsc.org
The design of porous sol–gel silica materials is a thriving research field, owing to silica's
diversity of properties and potential applications. Using a variety of additives, most …

A new insight into growth mechanism and kinetics of mesoporous silica nanoparticles by in situ small angle X-ray scattering

Z Yi, LF Dumée, CJ Garvey, C Feng, F She… - Langmuir, 2015 - ACS Publications
The growth mechanism and kinetics of mesoporous silica nanoparticles (MSNs) were
investigated for the first time by using a synchrotron time-resolved small-angle X-ray …

Cation-Induced Fibrillation of Microbial Glycolipid Biosurfactant Probed by Ion-Resolved In Situ SAXS

A Poirier, P Le Griel, J Perez… - The Journal of Physical …, 2022 - ACS Publications
Biological amphiphiles are molecules with a rich phase behavior. Micellar, vesicular, and
even fibrillar phases can be found for the same molecule by applying a change in pH or by …

Mechanisms of phase separation in temperature-responsive acidic aqueous biphasic systems

N Schaeffer, G Pérez-Sánchez, H Passos… - Physical Chemistry …, 2019 - pubs.rsc.org
The temperature responsive solubility of ionic liquids with 'bulky'polar regions, such as
tributyltetradecyl phosphonium chloride ([P44414] Cl), in acidic aqueous solutions is …

Tuning and controlling the shape of mesoporous silica particles with CTAB/sodium deoxycholate catanionic mixtures

L Travaglini, P Picchetti, A Del Giudice… - Microporous and …, 2019 - Elsevier
Controlling the shape and size of mesoporous silica particles (MSPs) requires a deep
understanding of the different parameters that play a major role during the synthesis of the …

Monodisperse mesoporous silica nanoparticles of distinct topology

L Luo, Y Liang, ES Erichsen, R Anwander - Journal of colloid and interface …, 2017 - Elsevier
Monodisperse and uniform high-quality MCM (Mobil Composition of Matter)-48-type CMSNs
(Cubic Mesoporous Silica Nanoparticles) are readily prepared by simply optimizing the …

A Small-Angle Neutron Scattering Environment for In-Situ Observation of Chemical Processes

DW Hayward, L Chiappisi, S Prévost, R Schweins… - Scientific Reports, 2018 - nature.com
A new sample environment for the observation of ongoing chemical reactions is introduced
for small-angle neutron scattering (SANS) experiments which enables structural changes to …

Nanoscale platelet formation by monounsaturated and saturated sophorolipids under basic pH conditions

AS Cuvier, F Babonneau, J Berton… - … A European Journal, 2015 - Wiley Online Library
The self‐assembly behavior of the yeast‐derived bolaamphiphile sophorolipid (SL) is
generally studied under acidic/neutral pH conditions, at which micellar and fibrillar …

An optimized protocol for the analysis of time-resolved elastic scattering experiments

MA Calabrese, NJ Wagner, SA Rogers - Soft Matter, 2016 - pubs.rsc.org
A deconvolution protocol is developed for obtaining material responses from time-resolved
small-angle scattering data from light (SALS), X-rays (SAXS), or neutrons (SANS) …