Spin hyperpolarization in modern magnetic resonance

J Eills, D Budker, S Cavagnero, EY Chekmenev… - Chemical …, 2023 - ACS Publications
Magnetic resonance techniques are successfully utilized in a broad range of scientific
disciplines and in various practical applications, with medical magnetic resonance imaging …

Primary structure of glycans by NMR spectroscopy

C Fontana, G Widmalm - Chemical reviews, 2023 - ACS Publications
Glycans, carbohydrate molecules in the realm of biology, are present as biomedically
important glycoconjugates and a characteristic aspect is that their structures in many …

Dynamic nuclear polarization for sensitivity enhancement in biomolecular solid-state NMR

T Biedenbänder, V Aladin, S Saeidpour… - Chemical …, 2022 - ACS Publications
Solid-state NMR with magic-angle spinning (MAS) is an important method in structural
biology. While NMR can provide invaluable information about local geometry on an atomic …

Overhauser enhanced liquid state nuclear magnetic resonance spectroscopy in one and two dimensions

M Levien, L Yang, A van der Ham, M Reinhard… - Nature …, 2024 - nature.com
Nuclear magnetic resonance (NMR) is fundamental in the natural sciences, from chemical
analysis and structural biology, to medicine and physics. Despite its enormous …

NMR methods for the analysis of mixtures

JN Dumez - Chemical Communications, 2022 - pubs.rsc.org
NMR spectroscopy is a powerful approach for the analysis of mixtures. Its usefulness arises
in large part from the vast landscape of methods, and corresponding pulse sequences, that …

Metal ions based dynamic nuclear polarization: MI-DNP

D Jardón-Álvarez, M Leskes - Progress in Nuclear Magnetic Resonance …, 2023 - Elsevier
Over the last two decades magic angle spinning dynamic nuclear polarization (MAS DNP)
has revolutionized NMR for materials characterization, tackling its main limitation of …

SHARPER-DOSY: Sensitivity enhanced diffusion-ordered NMR spectroscopy

G Peat, PJ Boaler, CL Dickson, GC Lloyd-Jones… - Nature …, 2023 - nature.com
Since its discovery in mid-20th century, the sensitivity of Nuclear Magnetic Resonance
(NMR) has increased steadily, in part due to the design of new, sophisticated NMR …

Polarizing agents beyond pentacene for efficient triplet dynamic nuclear polarization in glass matrices

K Sakamoto, T Hamachi, K Miyokawa… - Proceedings of the …, 2023 - pnas.org
Triplet dynamic nuclear polarization (triplet-DNP) is a technique that can obtain high nuclear
polarization under moderate conditions. However, in order to obtain practically useful …

Glycan shape, motions, and interactions explored by NMR spectroscopy

G Widmalm - JACS au, 2024 - ACS Publications
Glycans in the form of oligosaccharides, polysaccharides, and glycoconjugates are
ubiquitous in nature, and their structures range from linear assemblies to highly branched …

NMR investigations of glycan conformation, dynamics, and interactions

J Angulo, A Ardá, S Bertuzzi, A Canales… - Progress in Nuclear …, 2024 - Elsevier
Glycans are ubiquitous in nature, decorating our cells and serving as the initial points of
contact with any visiting entities. These glycan interactions are fundamental to host …