[HTML][HTML] Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR
ASL Thankamony, JJ Wittmann, M Kaushik… - Progress in nuclear …, 2017 - Elsevier
The field of dynamic nuclear polarization has undergone tremendous developments and
diversification since its inception more than 6 decades ago. In this review we provide an in …
diversification since its inception more than 6 decades ago. In this review we provide an in …
Solid-state NMR: Methods for biological solids
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
Facing and overcoming sensitivity challenges in biomolecular NMR spectroscopy
In the Spring of 2013, NMR spectroscopists convened at the Weizmann Institute in Israel to
brainstorm on approaches to improve the sensitivity of NMR experiments, particularly when …
brainstorm on approaches to improve the sensitivity of NMR experiments, particularly when …
Structural insights from lipid-bilayer nanodiscs link α-Synuclein membrane-binding modes to amyloid fibril formation
The protein α-Synuclein (αS) is linked to Parkinson's disease through its abnormal
aggregation, which is thought to involve cytosolic and membrane-bound forms of αS …
aggregation, which is thought to involve cytosolic and membrane-bound forms of αS …
DNP NMR of biomolecular assemblies
Abstract Dynamic Nuclear Polarization (DNP) is an effective approach to alleviate the
inherently low sensitivity of solid-state NMR (ssNMR) under magic angle spinning (MAS) …
inherently low sensitivity of solid-state NMR (ssNMR) under magic angle spinning (MAS) …
Solid-state dynamic nuclear polarization at 9.4 and 18.8 T from 100 K to room temperature
Efficient dynamic nuclear polarization (DNP) in solids, which enables very high sensitivity
NMR experiments, is currently limited to temperatures of around 100 K and below. Here we …
NMR experiments, is currently limited to temperatures of around 100 K and below. Here we …
Solid-state NMR on bacterial cells: selective cell wall signal enhancement and resolution improvement using dynamic nuclear polarization
Dynamic nuclear polarization (DNP) enhanced solid-state nuclear magnetic resonance
(NMR) has recently emerged as a powerful technique for the study of material surfaces. In …
(NMR) has recently emerged as a powerful technique for the study of material surfaces. In …
Efficient assignment and NMR analysis of an intact virus using sequential side-chain correlations and DNP sensitization
IV Sergeyev, B Itin, R Rogawski… - Proceedings of the …, 2017 - National Acad Sciences
An experimental strategy has been developed to increase the efficiency of dynamic nuclear
polarization (DNP) in solid-state NMR studies. The method makes assignments simpler …
polarization (DNP) in solid-state NMR studies. The method makes assignments simpler …
NMR-based structural biology enhanced by dynamic nuclear polarization at high magnetic field
EJ Koers, EAW van Der Cruijsen, M Rosay… - Journal of biomolecular …, 2014 - Springer
Dynamic nuclear polarization (DNP) has become a powerful method to enhance
spectroscopic sensitivity in the context of magnetic resonance imaging and nuclear …
spectroscopic sensitivity in the context of magnetic resonance imaging and nuclear …
Matrix-free dynamic nuclear polarization enables solid-state NMR 13 C–13 C correlation spectroscopy of proteins at natural isotopic abundance
We introduce a general approach for dynamic nuclear polarization (DNP) enhanced solid-
state NMR that overcomes the current problems in DNP experiments caused by the use of …
state NMR that overcomes the current problems in DNP experiments caused by the use of …