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Automated chemical oligosaccharide synthesis: novel approach to traditional challenges
Advances in carbohydrate chemistry have certainly made common oligosaccharides much
more accessible. However, many current methods still rely heavily upon specialized …
more accessible. However, many current methods still rely heavily upon specialized …
Recent advances in the analysis of complex glycoproteins
Notes 408 Biographies 408 Acknowledgments 409 References 409 The enormous
structural diversity of glycoconjugates mirrors their myriad biological functions in prokaryotic …
structural diversity of glycoconjugates mirrors their myriad biological functions in prokaryotic …
Recent liquid chromatographic approaches and developments for the separation and purification of carbohydrates
Carbohydrate purification remains a bottleneck in securing analytical standards from natural
sources or by chemical or enzymatic synthesis. This review highlights the scope and …
sources or by chemical or enzymatic synthesis. This review highlights the scope and …
Purification and concentration of minor impurity in the bulk drug by step-gradient twin-column recycling chromatography
F Wei, Y Hu, Y Zhao, Y Wu, G ** - Industrial & Engineering …, 2023 - ACS Publications
A weaker solvent was constantly added at the middle of the two columns to set up a two-step
solvent gradient in twin-column recycling chromatography so that the eluotropic strength of …
solvent gradient in twin-column recycling chromatography so that the eluotropic strength of …
Structural elucidation approaches in carbohydrates: A comprehensive review on techniques and future trends
Carbohydrates and their implications for human health have been the subject to a rapidly
growing interest. Substantial advances in analytical methods have enabled a more effective …
growing interest. Substantial advances in analytical methods have enabled a more effective …
HPLC‐Based Automated Synthesis of Glycans in Solution
As the 21st century unfolds with rapid changes, new challenges in research and
development emerge. These new challenges prompted us to repurpose our HPLC− A …
development emerge. These new challenges prompted us to repurpose our HPLC− A …
Recycling Preparative Liquid Chromatography, the Overlooked Methodology for the Purification of Natural Products
Frequently, preparative high-performance liquid chromatography separations of complex
natural product mixtures by adsorption chromatography are erratic to achieve full baseline …
natural product mixtures by adsorption chromatography are erratic to achieve full baseline …
Rebirth of recycling liquid chromatography with modern chromatographic columns: Extension to gradient elution
F Gritti - Journal of Chromatography A, 2021 - Elsevier
Twin column recycling semi-preparative liquid chromatography (TCRLC) is revived to
prepare small amount (∼ 1 mg) of a pure targeted compound, which cannot be isolated by …
prepare small amount (∼ 1 mg) of a pure targeted compound, which cannot be isolated by …
Power law approach as a convenient protocol for improving peak shapes and recovering areas from partially resolved peaks
Separation techniques have developed rapidly where sub-second chromatography,
ultrahigh resolution recycling chromatography, and two-dimensional liquid chromatography …
ultrahigh resolution recycling chromatography, and two-dimensional liquid chromatography …
Resolution limits of size exclusion chromatography columns identified from flow reversal and overcome by recycling liquid chromatography to improve the …
F Gritti - Journal of Chromatography A, 2023 - Elsevier
The flow reversal (FR) technique consists of reversing the flow direction along a
chromatographic column. It is used to reveal the origin (such as poor column packing, active …
chromatographic column. It is used to reveal the origin (such as poor column packing, active …