Dipolar recoupling in magic angle spinning solid-state nuclear magnetic resonance

G De Paëpe - Annual review of physical chemistry, 2012 - annualreviews.org
Solid-state nuclear magnetic resonance (SSNMR) magic angle spinning (MAS) can be used
to record high-resolution data dominated by site-specific information. Although MAS …

Recent progress in dipolar recoupling techniques under fast MAS in solid-state NMR spectroscopy

Y Ji, L Liang, X Bao, G Hou - Solid State Nuclear Magnetic Resonance, 2021 - Elsevier
With the recent advances in NMR hardware and probe design technology, magic-angle
spinning (MAS) rates over 100​ kHz are accessible now, even on commercial solid NMR …

Proton assisted recoupling and protein structure determination

G De Paëpe, JR Lewandowski, A Loquet… - The Journal of …, 2008 - pubs.aip.org
We introduce a homonuclear version of third spin assisted recoupling, a second-order
mechanism that can be used for polarization transfer between C 13 or N 15 spins in magic …

Dipolar truncation in magic-angle spinning NMR recoupling experiments

MJ Bayro, M Huber, R Ramachandran… - The Journal of …, 2009 - pubs.aip.org
Quantitative solid-state NMR distance measurements in strongly coupled spin systems are
often complicated due to the simultaneous presence of multiple noncommuting spin …

Solid-state NMR study of amyloid nanocrystals and fibrils formed by the peptide GNNQQNY from yeast prion protein Sup35p

PCA van der Wel, JR Lewandowski… - Journal of the American …, 2007 - ACS Publications
Sup35p is a prion protein found in yeast that contains a prion-forming domain characterized
by a repetitive sequence rich in Gln, Asn, Tyr, and Gly amino acid residues. The peptide …

Improved magnetization transfer in solid-state NMR with fast magic angle spinning

M Weingarth, DE Demco, G Bodenhausen… - Chemical Physics …, 2009 - Elsevier
The efficiency of magnetization transfer between different spins S such as chemically
inequivalent carbon-13 nuclei in solid samples that are spinning at high frequencies about …

Solid-state NMR studies of HIV-1 capsid protein assemblies

Y Han, J Ahn, J Concel, IJL Byeon… - Journal of the …, 2010 - ACS Publications
In mature HIV-1 virions, the 26.6 kDa CA protein is assembled into a characteristic cone-
shaped core (capsid) that encloses the RNA viral genome. The assembled capsid structure …

1H–13C/1H–15N Heteronuclear Dipolar Recoupling by R-Symmetry Sequences Under Fast Magic Angle Spinning for Dynamics Analysis of Biological and …

G Hou, IJL Byeon, J Ahn, AM Gronenborn… - Journal of the …, 2011 - ACS Publications
Fast magic angle spinning (MAS) NMR spectroscopy is becoming increasingly important in
structural and dynamics studies of biological systems and inorganic materials. Superior …

Measurement of Site-Specific 13C Spin−Lattice Relaxation in a Crystalline Protein

JR Lewandowski, J Sein, HJ Sass… - Journal of the …, 2010 - ACS Publications
We demonstrate that it is possible to record site-specific spin− lattice relaxation rates for the
majority of 13C sites in uniformly 13C and 15N labeled solid proteins as a result of the …

[HTML][HTML] NMR structural studies of the antibiotic lipopeptide daptomycin in DHPC micelles

WRP Scott, SB Baek, D Jung, REW Hancock… - … et Biophysica Acta (BBA …, 2007 - Elsevier
Daptomycin is a cyclic anionic lipopeptide that exerts its rapid bactericidal effect by
perturbing the bacterial cell membrane, a mode of action different from most other currently …