High-resolution native mass spectrometry

S Tamara, MA den Boer, AJR Heck - Chemical reviews, 2021‏ - ACS Publications
Native mass spectrometry (MS) involves the analysis and characterization of
macromolecules, predominantly intact proteins and protein complexes, whereby as much as …

Mass spectrometry-based protein footprinting for higher-order structure analysis: fundamentals and applications

XR Liu, MM Zhang, ML Gross - Chemical reviews, 2020‏ - ACS Publications
Proteins adopt different higher-order structures (HOS) to enable their unique biological
functions. Understanding the complexities of protein higher-order structures and dynamics …

Protein–small molecule interactions in native mass spectrometry

JL Bennett, GTH Nguyen, WA Donald - Chemical Reviews, 2021‏ - ACS Publications
Small molecule drug discovery has been propelled by the continual development of novel
scientific methodologies to occasion therapeutic advances. Although established …

Carbonic anhydrase inhibitors targeting metabolism and tumor microenvironment

A Angeli, F Carta, A Nocentini, JY Winum… - Metabolites, 2020‏ - mdpi.com
The tumor microenvironment is crucial for the growth of cancer cells, triggering particular
biochemical and physiological changes, which frequently influence the outcome of …

Rapid online buffer exchange for screening of proteins, protein complexes and cell lysates by native mass spectrometry

ZL VanAernum, F Busch, BJ Jones, M Jia, Z Chen… - Nature protocols, 2020‏ - nature.com
It is important to assess the identity and purity of proteins and protein complexes during and
after protein purification to ensure that samples are of sufficient quality for further …

Reconsidering anion inhibitors in the general context of drug design studies of modulators of activity of the classical enzyme carbonic anhydrase

A Nocentini, A Angeli, F Carta, JY Winum… - Journal of Enzyme …, 2021‏ - Taylor & Francis
Inorganic anions inhibit the metalloenzyme carbonic anhydrase (CA, EC 4.2. 1.1) generally
by coordinating to the active site metal ion. Cyanate was reported as a non-coordinating CA …

Studying protein structure and function by native separation–mass spectrometry

G van Schaick, R Haselberg, GW Somsen… - Nature Reviews …, 2022‏ - nature.com
Alterations in protein structure may have profound effects on biological function. Analytical
techniques that permit characterization of proteins while maintaining their conformational …

Experimental carbonic anhydrase inhibitors for the treatment of hypoxic tumors

CT Supuran - Journal of Experimental Pharmacology, 2020‏ - Taylor & Francis
Abstract Carbonic anhydrase (CA, EC 4.2. 1.1) isoforms IX and XII are overexpressed in
many hypoxic tumors as a consequence of the hypoxia inducible factor (HIF) activation …

Approaches to heterogeneity in native mass spectrometry

AD Rolland, JS Prell - Chemical reviews, 2021‏ - ACS Publications
Native mass spectrometry (MS) is aimed at preserving and determining the native structure,
composition, and stoichiometry of biomolecules and their complexes from solution after they …

On the chemistry of aqueous ammonium acetate droplets during native electrospray ionization mass spectrometry

L Konermann, Z Liu, Y Haidar, MJ Willans… - Analytical …, 2023‏ - ACS Publications
Ammonium acetate (NH4Ac) is a widely used solvent additive in native electrospray
ionization (ESI) mass spectrometry. NH4Ac can undergo proton transfer to form ammonia …