In-situ multi-phase flow imaging for particle dynamic tracking and characterization: Advances and applications

J Liu, W Kuang, J Liu, Z Gao, S Rohani… - Chemical Engineering …, 2022 - Elsevier
Real-time chemical process monitoring, analysis, and control have become increasingly
important to multi-phase flow process research and development and attracted overt …

[HTML][HTML] Application of PAT-based feedback control approaches in pharmaceutical crystallization

Y Gao, T Zhang, Y Ma, F Xue, Z Gao, B Hou, J Gong - Crystals, 2021 - mdpi.com
Crystallization is one of the important unit operations for the separation and purification of
solid products in the chemical, pharmaceutical, and pesticide industries, especially for …

Progress to date in the design and operation of continuous crystallization processes for pharmaceutical applications

B Wood, KP Girard, CS Polster… - … Process Research & …, 2019 - ACS Publications
Continuous crystallization has gained interest in the pharmaceutical sector as part of the
drive toward the transition from exclusive batch manufacturing to integrated continuous …

Recent progress in continuous crystallization of pharmaceutical products: precise preparation and control

Y Ma, S Wu, EGJ Macaringue, T Zhang… - … Process Research & …, 2020 - ACS Publications
Crystallization, as a solid–liquid separation process, is employed to purify and isolate a
great diversity of crystalline pharmaceutical products. In recent years, continuous …

Impurity incorporation in solution crystallization: diagnosis, prevention, and control

G Capellades, JO Bonsu, AS Myerson - CrystEngComm, 2022 - pubs.rsc.org
Despite their widespread use for purification, our current methods for the development of
solution crystallization processes lack a sufficient understanding on how impurities …

Prevalence of impurity retention mechanisms in pharmaceutical crystallizations

FL Nordstrom, E Sirota, C Hartmanshenn… - … Process Research & …, 2023 - ACS Publications
The rejection of process impurities from crystallizing products is an essential step for the
purification of pharmaceutical drugs and for the isolation of active pharmaceutical …

Tuning crystal morphology of succinic acid using a polymer additive

AR Klapwijk, E Simone, ZK Nagy… - Crystal Growth & …, 2016 - ACS Publications
The effect of the triblock copolymer Pluronic P123 (PP123) on the growth of succinic acid
crystals from aqueous solutions is reported at two batch process scales: 10 and 350 mL. The …

Monitoring and digital design of the cooling crystallization of a high-aspect ratio anticancer drug using a two-dimensional population balance model

B Szilágyi, A Eren, JL Quon, CD Papageorgiou… - Chemical Engineering …, 2022 - Elsevier
The development of a process model for the batch cooling crystallization of an anticancer
drug from Takeda Pharmaceuticals is presented. The compound forms needle-like crystals …

Mechanisms and control of impurities in continuous crystallization: a review

C Darmali, S Mansouri, N Yazdanpanah… - Industrial & …, 2018 - ACS Publications
Crystallization has been applied to a broad range of industries such as bulk and fine
chemicals and the pharmaceutical and food industries. It is important to strategically control …

[HTML][HTML] Image analysis framework with focus evaluation for in situ characterisation of particle size and shape attributes

J Cardona, C Ferreira, J McGinty, A Hamilton… - Chemical Engineering …, 2018 - Elsevier
Particle processing industries, such as pharmaceutical, food processing and consumer
goods sectors, increasingly require strategies to control and engineer particle attributes. In …