Recent advances in stable main group element radicals: preparation and characterization

Z Feng, S Tang, Y Su, X Wang - Chemical Society Reviews, 2022 - pubs.rsc.org
Radical species are significant in modern chemistry. Their unique chemical bonding and
novel physicochemical properties play significant roles not only in fundamental chemistry …

Heavier group 13/15 multiple bond systems: synthesis, structure and chemical bond activation

F Dankert, C Hering-Junghans - Chemical Communications, 2022 - pubs.rsc.org
Heavier group 13/15 multiple bonds have been under investigation since the late 80s and to
date, several examples have been published, which shows the obsoleteness of the so …

Thorium(iv)–antimony complexes exhibiting single, double, and triple polar covalent metal–metal bonds

J Du, K Dollberg, JA Seed, AJ Wooles… - Nature Chemistry, 2024 - nature.com
There is continued burgeoning interest in metal–metal multiple bonding to further our
understanding of chemical bonding across the periodic table. However, although polar …

Multi‐Talented Gallaphosphene for Ga−P−Ga Heteroallyl Cation Generation, CO2 Storage, and C(sp3)−H Bond Activation

MK Sharma, C Wölper, G Haberhauer… - Angewandte Chemie …, 2021 - Wiley Online Library
Abstract Gallaphosphene L (Cl) GaPGaL (2; L= HC [C (Me) N (2, 6‐i‐Pr2C6H3)] 2), which is
synthesized by reaction of LGa (Cl) PCO (1) with LGa, reacts with [Na (OCP)(dioxane) 2.5] to …

Synthesis, structure and bonding nature of heavy dipnictene radical anions

HM Weinert, C Wölper, J Haak, GE Cutsail… - Chemical Science, 2021 - pubs.rsc.org
Cyclic voltammetry (CV) studies of two L (X) Ga-substituted dipnictenes [L (R2N) GaE] 2 (E=
Sb, R= Me 1; E= Bi; R= Et 2; L= HC [C (Me) NDipp] 2; Dipp= 2, 6-i-Pr2C6H3) showed …

Stepwise Bi–Bi Bond Formation: From a Bi-centered Radical to Bi4 Butterfly and Bi8 Cuneane-Type Clusters

J Krüger, C Wölper, S Schulz - Inorganic Chemistry, 2020 - ACS Publications
In contrast to their lighter homologues (P, As, Sb), the synthesis of polybismuthane clusters
is still restricted to classical solid-state approaches. We herein report on systematic …

Reversible and Irreversible [2+ 2] Cycloaddition Reactions of Heteroallenes to a Gallaphosphene

MK Sharma, C Wölper, G Haberhauer… - Angewandte Chemie …, 2021 - Wiley Online Library
Cycloaddition reactions of gallaphosphene L (Cl) GaPGaL 1 (L= HC [C (Me) N (2, 6‐i‐
Pr2C6H3)] 2) with carbodiimides [C (NR) 2; R= i‐Pr, Cy] and isocyanates [RNCO; R= Et, i …

Applications of electron paramagnetic resonance spectroscopy to heavy main-group radicals

GE Cutsail - Dalton Transactions, 2020 - pubs.rsc.org
The exploration of heavy main-group radicals is rapidly expanding, for which electron
paramagnetic resonance (EPR) spectroscopic characterisation plays a key role. EPR …

Ligand effects on the electronic structure of heteroleptic antimony‐centered radicals

C Helling, GE Cutsail III, H Weinert… - Angewandte …, 2020 - Wiley Online Library
We report on the structures of three unprecedented heteroleptic Sb‐centered radicals [L (Cl)
Ga](R) Sb.(2‐R, R= B [N (Dip) CH] 2 2‐B, 2, 6‐Mes2C6H3 2‐C, N (SiMe3) Dip 2‐N) …

Selective 1, 2 addition of polar X–H bonds to the Ga–P double bond of gallaphosphene L (Cl) GaPGaL

MK Sharma, C Wölper, S Schulz - Dalton Transactions, 2022 - pubs.rsc.org
Gallaphosphene L (Cl) GaPGaL 1 (L= HC [C (Me) N (2, 6-i-Pr2-C6H3)] 2) reacts at ambient
temperature with a series of polar X–H bonds, ie ammonia, primary amines, water, phenol …