Dipolar Recoupling in Rotating Solids
Magic angle spinning (MAS) nuclear magnetic resonance (NMR) has evolved significantly
over the past three decades and established itself as a vital tool for the structural analysis of …
over the past three decades and established itself as a vital tool for the structural analysis of …
Floquet theory in magnetic resonance: Formalism and applications
Floquet theory is an elegant mathematical formalism originally developed to solve time-
dependent differential equations. Besides other fields, it has found applications in optical …
dependent differential equations. Besides other fields, it has found applications in optical …
Simplified Preservation of Equivalent Pathways Spectroscopy
E Nimerovsky, AC Varkey, M Kim, S Becker… - JACS Au, 2023 - ACS Publications
Inspired by the recently proposed transverse mixing optimal control pulses (TROP)
approach for improving signal in multidimensional magic-angle spinning (MAS) NMR …
approach for improving signal in multidimensional magic-angle spinning (MAS) NMR …
[HTML][HTML] Windowed cross polarization at 55 kHz magic-angle spinning
Cross polarization (CP) transfers via Hartmann-Hahn matching conditions are one of the
cornerstones of solid-state magic-angle spinning NMR experiments. Here we investigate a …
cornerstones of solid-state magic-angle spinning NMR experiments. Here we investigate a …
Deuteron-proton isotope correlation spectroscopy at high magnetic fields
A cross-polarization-based 2 H-1 H isotope correlation spectroscopy (CP-iCOSY) approach
is presented for characterizing deuterated amino acids, pharmaceutical compounds and a …
is presented for characterizing deuterated amino acids, pharmaceutical compounds and a …
Homonuclear J-couplings and heteronuclear structural constraints
In magic angle spinning (MAS) experiments involving uniformly 13 C/15 N labeled proteins,
13 C–13 C and 13 C–15 N dipolar recoupling experiments are now routinely used to …
13 C–13 C and 13 C–15 N dipolar recoupling experiments are now routinely used to …
A general theoretical description of the influence of isotropic chemical shift in dipolar recoupling experiments for solid-state NMR
We present a general theoretical description that allows us to describe the influence of
isotropic chemical shift in homonuclear and heteronuclear dipolar recoupling experiments in …
isotropic chemical shift in homonuclear and heteronuclear dipolar recoupling experiments in …
Efficient 15N–13C Polarization Transfer by Third-Spin-Assisted Pulsed Cross-Polarization Magic-Angle-Spinning NMR for Protein Structure Determination
We introduce a pulsed third-spin-assisted recoupling experiment that produces high-
intensity long-range 15N–13C cross peaks using low radiofrequency (rf) energy. This Proton …
intensity long-range 15N–13C cross peaks using low radiofrequency (rf) energy. This Proton …
Band-selective heteronuclear dipolar recoupling with dual back-to-back pulses in rotating solids
Z Zhang, Y Chen, J Yang - Journal of Magnetic Resonance, 2016 - Elsevier
We propose a robust band-selective heteronuclear 15 N-13 C recoupling method using dual
back-to-back (BABA) pulses (DBP). It contains four 90° pulses in each rotor period and …
back-to-back (BABA) pulses (DBP). It contains four 90° pulses in each rotor period and …
A robust heteronuclear dipolar recoupling method comparable to TEDOR for proteins in magic-angle spinning solid-state NMR
In this letter, we propose a robust heteronuclear dipolar recoupling method for proteins in
magic-angle spinning (MAS) solid-state NMR. This method is as simple, robust and efficient …
magic-angle spinning (MAS) solid-state NMR. This method is as simple, robust and efficient …