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1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning
T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …
ago, 1H detection has evolved into the most efficient approach for investigation of …
[HTML][HTML] Paramagnetic NMR in solution and the solid state
The field of paramagnetic NMR has expanded considerably in recent years. This review
addresses both the theoretical description of paramagnetic NMR, and the way in which it is …
addresses both the theoretical description of paramagnetic NMR, and the way in which it is …
Paramagnetic chemical probes for studying biological macromolecules
Paramagnetic chemical probes have been used in electron paramagnetic resonance (EPR)
and nuclear magnetic resonance (NMR) spectroscopy for more than four decades. Recent …
and nuclear magnetic resonance (NMR) spectroscopy for more than four decades. Recent …
NMR crystallography of molecular organics
P Hodgkinson - Progress in Nuclear Magnetic Resonance …, 2020 - Elsevier
Developments of NMR methodology to characterise the structures of molecular organic
structures are reviewed, concentrating on the previous decade of research in which density …
structures are reviewed, concentrating on the previous decade of research in which density …
Imaging active site chemistry and protonation states: NMR crystallography of the tryptophan synthase α-aminoacrylate intermediate
NMR-assisted crystallography—the integrated application of solid-state NMR, X-ray
crystallography, and first-principles computational chemistry—holds significant promise for …
crystallography, and first-principles computational chemistry—holds significant promise for …
The evolution of paramagnetic NMR as a tool in structural biology
Paramagnetic NMR data contain extremely accurate long-range information on
metalloprotein structures and, when used in the frame of integrative structural biology …
metalloprotein structures and, when used in the frame of integrative structural biology …
NMR crystallography of a carbanionic intermediate in tryptophan synthase: chemical structure, tautomerization, and reaction specificity
Carbanionic intermediates play a central role in the catalytic transformations of amino acids
performed by pyridoxal-5′-phosphate (PLP)-dependent enzymes. Here, we make use of …
performed by pyridoxal-5′-phosphate (PLP)-dependent enzymes. Here, we make use of …
Picometer resolution structure of the coordination sphere in the metal-binding site in a metalloprotein by NMR
Most of our understanding of chemistry derives from atomic-level structures obtained with
single-crystal X-ray diffraction. Metal centers in X-ray structures of small organometallic or …
single-crystal X-ray diffraction. Metal centers in X-ray structures of small organometallic or …
Determination of the electronic and structural configuration of coordination compounds by synchrotron-radiation techniques
In this review we provide an overview of the potential of synchrotron radiation techniques to
understand the structural and electronic properties of coordination compounds. Besides the …
understand the structural and electronic properties of coordination compounds. Besides the …
Structure determination of protein–protein complexes with long-range anisotropic paramagnetic NMR restraints
MAS Hass, M Ubbink - Current opinion in structural biology, 2014 - Elsevier
Highlights•Anisotropic paramagnetic effects include PseudoContact Shifts and RDC.•PCS
provide long-range restraints for structure determination.•Practical aspects of PCS structure …
provide long-range restraints for structure determination.•Practical aspects of PCS structure …