Heteronuclear spin decoupling is a vital element in most of the solid‐state nuclear magnetic
resonance experiments for resolution and sensitivity reasons. The field has seen remarkable …

Recent structural studies show distinct morphologies for the fibrils of Aβ (1–42) and Aβ (1–
40), which are believed not to co-fibrillize. We describe here a novel, structurally-uniform 1: 1 …

Reliable methods for the characterization of drug substances are critical for evaluating
stability and bioavailability, especially in dosage formulations under varying storage …

We describe a simple yet highly effective optimization strategy for SPINAL-64 1H decoupling
conditions for magic-angle spinning solid-state NMR. With adjustment of the phase angles in …

Variable-hydrate active pharmaceutical ingredients (APIs) are known to form
thermodynamically and kinetically stabilized solid phases over a continuous range of …

Silica nanoparticles can be designed to exhibit a diverse range of morphologies (eg non-
porous, mesoporous), physical properties (eg hydrophobic, hydrophilic) and a wide range of …

The 15 N chemical shift tensor is shown to be extremely sensitive to lattice structure and a
powerful metric for monitoring density functional theory refinements of crystal structures …

Apremilast (APR), an anti-psoriatic agent, easily forms isostructural cocrystals and solvates
with aromatic entities, often disobeying at the same time Kitaigorodsky's rule as to the …

Among protein immobilization strategies, encapsulation in bioinspired silica is increasingly
popular. Encapsulation offers high yields and the solid support is created through a protein …

In solid-state nuclear magnetic resonance (SSNMR) under magic-angle spinning (MAS), the
dipolar interactions (that contains distance information), averaged out by sample spinning …