Solid-state 17O NMR studies of organic and biological molecules

G Wu - Progress in Nuclear Magnetic Resonance …, 2008 - Elsevier
Oxygen (O), hydrogen (H), carbon (C), and nitrogen (N) are the most common elements
found in organic and biological molecules. Among these four elements, oxygen occupies a …

High-resolution NMR of quadrupolar nuclei in solids: the satellite-transition magic angle spinning (STMAS) experiment

SE Ashbrook, S Wimperis - Progress in Nuclear Magnetic Resonance …, 2004 - Elsevier
1. Introduction............................................................................. 54 2. Theoretical
background.................................................................... 55 2.1. Origin of quadrupolar …

Structural information from quadrupolar nuclei in solid state NMR

SE Ashbrook, MJ Duer - … in Magnetic Resonance Part A: An …, 2006 - Wiley Online Library
Solid‐state NMR has become the method of choice for determining details of molecular‐
level structure in heterogeneous systems. Though spin‐1/2 nuclei still form the core of most …

Cogwheel phase cycling

MH Levitt, PK Madhu, CE Hughes - Journal of Magnetic Resonance, 2002 - Elsevier
A new method for constructing phase cycles is described. The new schemes apply to
experiments involving several consecutive coherence transfer steps. The radiofrequency …

Correlated structural distributions in silica glass

TM Clark, PJ Grandinetti, P Florian, JF Stebbins - Physical Review B …, 2004 - APS
The two-dimensional O 17 dynamic-angle spinning solid-state nuclear magnetic resonance
spectrum of silica glass produced from the melt was measured. From this spectrum a three …

27Al NMR studies of aluminosilicate glasses

M Eden - Annual Reports on NMR Spectroscopy, 2015 - Elsevier
Aluminosilicate glasses are of great geological and technological importance. Significant
efforts have been spent for enhancing the insight into their structures, where magic-angle …

Update on 27Al NMR studies of aluminosilicate glasses

M Eden - Annual reports on NMR spectroscopy, 2020 - Elsevier
Aluminosilicate glasses and melts are of great geological and technological importance.
Significant efforts have been spent for enhancing the insight into their structures. Here magic …

Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers

HT Kwak, S Prasad, T Clark, PJ Grandinetti - Solid state nuclear magnetic …, 2003 - Elsevier
Rotor-assisted population transfer (RAPT) was developed as a method for enhancing MAS
NMR sensitivity of quadrupolar nuclei by transferring polarization associated with satellite …

HMQC and refocused-INEPT experiments involving half-integer quadrupolar nuclei in solids

JP Amoureux, J Trebosc, J Wiench, M Pruski - Journal of magnetic …, 2007 - Elsevier
Hetero-nuclear coherence transfers in HMQC and refocused-INEPT experiments involving
half-integer quadrupolar nuclei in solids are analyzed. 1D and 2D schemes are considered …

Probing quadrupolar nuclei by solid-state NMR spectroscopy: recent advances

C Fernandez, M Pruski - Solid State NMR, 2012 - Springer
Solid-state nuclear magnetic resonance (NMR) of quadrupolar nuclei has recently
undergone remarkable development of capabilities for obtaining structural and dynamic …