Reactivity of surface species in heterogeneous catalysts probed by in situ X-ray absorption techniques

S Bordiga, E Groppo, G Agostini… - Chemical …, 2013 - ACS Publications
Starting from the late seventies, the progressively increased availability of synchrotron light
sources allowed the execution of experiments requiring a high X-ray flux in a continuous …

Porous aluminophosphates: from molecular sieves to designed acid catalysts

HO Pastore, S Coluccia, L Marchese - Annu. Rev. Mater. Res., 2005 - annualreviews.org
▪ Abstract This review covers the synthesis, characterization, and physico-chemical
properties of microporous and mesoporous aluminophosphates and …

Consequences of confinement for alkene epoxidation with hydrogen peroxide on highly dispersed group 4 and 5 metal oxide catalysts

DT Bregante, NE Thornburg, JM Notestein… - Acs …, 2018 - ACS Publications
Ti, Nb, and Ta atoms substituted into the framework of zeolite* BEA (M-BEA) or grafted onto
mesoporous silica (M-SiO2) irreversibly activate hydrogen peroxide (H2O2) to form pools of …

Periodic trends in olefin epoxidation over group IV and V framework-substituted zeolite catalysts: a kinetic and spectroscopic study

DT Bregante, DW Flaherty - Journal of the American Chemical …, 2017 - ACS Publications
Group IV and V framework-substituted zeolites have been used for olefin epoxidation
reactions for decades, yet the underlying properties that determine the selectivities and …

Alkene Epoxidations with H2O2 over Groups 4–6 Metal-Substituted BEA Zeolites: Reactive Intermediates, Reaction Pathways, and Linear Free-Energy …

EZ Ayla, DS Potts, DT Bregante, DW Flaherty - ACS Catalysis, 2020 - ACS Publications
Rates and selectivities for alkene epoxidations depend sensitively on the identity of the
active metal center for both heterogeneous and homogeneous catalysts. While group 6 …

Selective oxidation of furfural to succinic acid over lewis acidic Sn-beta

YN Palai, A Shrotri, A Fukuoka - ACS catalysis, 2022 - ACS Publications
Selective production of succinic acid from furfural with H2O2 over Sn-Beta, a pure Lewis
acid catalyst, is reported. Under optimized reaction conditions, 53% yield of succinic acid …

Evidence of defect-promoted reactivity for epoxidation of propylene in titanosilicate (TS-1) catalysts: a DFT study

DH Wells Jr, WN Delgass Jr… - Journal of the American …, 2004 - ACS Publications
Our density functional theory study of hydroperoxy (OOH) intermediates on various model
titanosilicalite (TS-1) Ti centers explores how microstructural aspects of Ti sites effect …

Reactivity of Ti (iv) species hosted in TS-1 towards H 2 O 2–H 2 O solutions investigated by ab initio cluster and periodic approaches combined with experimental …

S Bordiga, F Bonino, A Damin… - Physical Chemistry …, 2007 - pubs.rsc.org
This work is intended to underline how the most-advanced experimental and theoretical
physical chemistry tools must be used synergistically to understand the reactivity of Ti …

Heterogeneous Catalytic Oxidation of As(III) on Nonferrous Metal Oxides in the Presence of H2O2

D Kim, AD Bokare, MS Koo, W Choi - Environmental Science & …, 2015 - ACS Publications
The oxidation of As (III)(arsenite) to As (V)(arsenate), a critical pretreatment process for total
arsenic removal, is easily achieved using chemical oxidation methods. Hydrogen peroxide …

Transient technique for identification of true reaction intermediates: Hydroperoxide species in propylene epoxidation on gold/titanosilicate catalysts by X-ray …

JJ Bravo-Suárez, KK Bando, J Lu… - The Journal of …, 2008 - ACS Publications
In situ ultraviolet− visible (UV− vis) diffuse reflectance spectroscopy was used in
combination with in situ Ti K-edge X-ray absorption near-edge structure (XANES) to study …