Recent advances in solid-state nuclear magnetic resonance spectroscopy of exotic nuclei

C Leroy, DL Bryce - Progress in Nuclear Magnetic Resonance …, 2018 - Elsevier
We present a review of recent advances in solid-state nuclear magnetic resonance
(SSNMR) studies of exotic nuclei. Exotic nuclei may be spin-1/2 or quadrupolar, and …

Recent progress in solid‐state nuclear magnetic resonance of half‐integer spin low‐γ quadrupolar nuclei applied to inorganic materials

ME Smith - Magnetic Resonance in Chemistry, 2021 - Wiley Online Library
An overview is presented of recent progress in the solid‐state nuclear magnetic resonance
(NMR) observation of low‐γ nuclei, with a focus on applications to inorganic materials. The …

Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy

D Lee, C Leroy, C Crevant, L Bonhomme-Coury… - Nature …, 2017 - nature.com
The interfaces within bones, teeth and other hybrid biomaterials are of paramount
importance but remain particularly difficult to characterize at the molecular level because …

Direct 17 O dynamic nuclear polarization of single-site heterogeneous catalysts

FA Perras, KC Boteju, II Slowing, AD Sadow… - Chemical …, 2018 - pubs.rsc.org
We utilize direct 17O DNP for the characterization of non-protonated oxygens in
heterogeneous catalysts. The optimal sample preparation and population transfer approach …

A facile approach for estimating radio-frequency field strength of low-receptivity nuclei

NT Duong, S Viel, F Ziarelli, P Thureau… - Journal of Magnetic …, 2024 - Elsevier
Radio-frequency (RF) field calibration is essential in NMR spectroscopy. A common practice
is to collect a nutation curve by varying the pulse length in a direct single-pulse excitation …

Pushing the limits of sensitivity and resolution for natural abundance 43 Ca NMR using ultra-high magnetic field (35.2 T)

C Bonhomme, X Wang, I Hung, Z Gan… - Chemical …, 2018 - pubs.rsc.org
Natural abundance 43Ca solid state NMR experiments are reported for the first time at ultra-
high magnetic field (35.2 T) on a series of Ca-(pyro) phosphate and Ca-oxalate materials …

Loading across the periodic table: introducing 14 different metal ions to enhance metal–organic framework performance

S Chen, BEG Lucier, W Luo, X **
I Hung, AR Altenhof, RW Schurko… - Magnetic …, 2021 - Wiley Online Library
Field‐stepped NMR spectroscopy at up to 36 T using the series‐connected hybrid (SCH)
magnet at the US National High Magnetic Field Laboratory is demonstrated for acquiring …

43Ca MAS-DNP NMR of Frozen Solutions for the Investigation of Calcium Ion Complexation

T Georges, R Chèvre, SF Cousin, C Gervais… - ACS …, 2024 - ACS Publications
Calcium ion complexation in aqueous solutions is of paramount importance in biology as it
is related to cell signaling, muscle contraction, or biomineralization. However, Ca2+ …