Toward autonomous design and synthesis of novel inorganic materials

NJ Szymanski, Y Zeng, H Huo, CJ Bartel, H Kim… - Materials …, 2021 - pubs.rsc.org
Autonomous experimentation driven by artificial intelligence (AI) provides an exciting
opportunity to revolutionize inorganic materials discovery and development. Herein, we …

Combinatorial synthesis for AI-driven materials discovery

JM Gregoire, L Zhou, JA Haber - Nature Synthesis, 2023 - nature.com
Combinatorial synthesis of solid-state materials comprises the use of automation or
parallelization to systematically vary synthesis parameters. This approach to materials …

Progress and prospects for accelerating materials science with automated and autonomous workflows

HS Stein, JM Gregoire - Chemical science, 2019 - pubs.rsc.org
Accelerating materials research by integrating automation with artificial intelligence is
increasingly recognized as a grand scientific challenge to discover and develop materials …

Autonomous materials synthesis via hierarchical active learning of nonequilibrium phase diagrams

S Ament, M Amsler, DR Sutherland, MC Chang… - Science …, 2021 - science.org
Autonomous experimentation enabled by artificial intelligence offers a new paradigm for
accelerating scientific discovery. Nonequilibrium materials synthesis is emblematic of …

Thin-film processing routes for combinatorial materials investigations—a review

PJ McGinn - ACS Combinatorial Science, 2019 - ACS Publications
High-throughput combinatorial investigations are transforming materials discovery, phase
diagram development, and processing optimization. Thin-film deposition techniques are …

Block copolymer self-assembly directed hierarchically structured materials from nonequilibrium transient laser heating

KW Tan, U Wiesner - Macromolecules, 2019 - ACS Publications
We highlight two recent approaches operating far from equilibrium for the synthesis of
hierarchical porous thin film materials by coupling block copolymer-directed self-assembly …

Macroscopic alignment of block copolymers on silicon substrates by laser annealing

AA Leniart, P Pula, A Sitkiewicz, PW Majewski - ACS nano, 2020 - ACS Publications
Laser annealing is a competitive alternative to conventional oven annealing of block
copolymer (BCP) thin films enabling rapid acceleration and precise spatial control of the self …

Ultrafast self-assembly of sub-10 nm block copolymer nanostructures by solvent-free high-temperature laser annealing

J Jiang, AG Jacobs, B Wenning, C Liedel… - … applied materials & …, 2017 - ACS Publications
Laser spike annealing was applied to PS-b-PDMS diblock copolymers to induce short-time
(millisecond time scale), high-temperature (300 to 700° C) microphase segregation and …

Laser writing of electronic circuitry in thin film molybdenum disulfide: A transformative manufacturing approach

D Austin, K Gliebe, C Muratore, B Boyer, TS Fisher… - Materials Today, 2021 - Elsevier
Electronic circuits, the backbone of modern electronic devices, require precise integration of
conducting, insulating, and semiconducting materials in two-and three-dimensional space to …

[HTML][HTML] Initial nucleation of metastable γ-Ga2O3 during sub-millisecond thermal anneals of amorphous Ga2O3

KR Gann, CS Chang, MC Chang… - Applied Physics …, 2022 - pubs.aip.org
Beta-phase gallium oxide (⁠ β-Ga 2 O 3) is a promising semiconductor for high frequency,
high temperature, and high voltage applications. In addition to the β-phase, numerous other …