Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning

T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …

Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

Bacterial membrane transporter systems for aromatic compounds: regulation, engineering, and biotechnological applications

I Mutanda, J Sun, J Jiang, D Zhu - Biotechnology advances, 2022 - Elsevier
Aromatic compounds are ubiquitous in nature; they are the building blocks of abundant
lignin, and constitute a substantial proportion of synthetic chemicals and organic pollutants …

Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems

L Liang, Y Ji, K Chen, P Gao, Z Zhao, G Hou - Chemical reviews, 2022 - ACS Publications
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

From angstroms to nanometers: measuring interatomic distances by solid-state NMR

AA Shcherbakov, J Medeiros-Silva, N Tran… - Chemical …, 2021 - ACS Publications
Internuclear distances represent one of the main structural constraints in molecular structure
determination using solid-state NMR spectroscopy, complementing chemical shifts and …

Mechanism of high Li-ion conductivity in poly (vinylene carbonate)-poly (ethylene oxide) cross-linked network based electrolyte revealed by solid-state NMR

F Li, T Dong, Y Ji, L Liang, K Chen, H Zhang… - Journal of Energy …, 2024 - Elsevier
Solid polymer electrolytes (SPEs) have become increasingly important in advanced lithium-
ion batteries (LIBs) due to their improved safety and mechanical properties compared to …

Sensitivity-enhanced multidimensional solid-state NMR spectroscopy by optimal-control-based transverse mixing sequences

J Blahut, MJ Brandl, T Pradhan, B Reif… - Journal of the …, 2022 - ACS Publications
Recently, proton-detected magic-angle spinning (MAS) solid-state nuclear magnetic
resonance (NMR) spectroscopy has become an attractive tool to study the structure and …

Atomic-resolution chemical characterization of (2x)72-kDa tryptophan synthase via four- and five-dimensional 1H-detected solid-state NMR

A Klein, P Rovó, VV Sakhrani, Y Wang… - Proceedings of the …, 2022 - pnas.org
NMR chemical shifts provide detailed information on the chemical properties of molecules,
thereby complementing structural data from techniques like X-ray crystallography and …

Deuteration for high-resolution detection of protons in protein magic angle spinning (MAS) solid-state NMR

B Reif - Chemical Reviews, 2021 - ACS Publications
Proton detection developed in the last 20 years as the method of choice to study
biomolecules in the solid state. In perdeuterated proteins, proton dipolar interactions are …