Progress in uranium chemistry: driving advances in front-end nuclear fuel cycle forensics

KJ Pastoor, RS Kemp, MP Jensen… - Inorganic Chemistry, 2021 - ACS Publications
The front-end of the nuclear fuel cycle encompasses several chemical and physical
processes used to acquire and prepare uranium for use in a nuclear reactor. These same …

The Role of Alkalis in Orchestrating Uranyl‐Peroxide Reactivity Leading to Direct Air Capture of Carbon Dioxide

A Arteaga, T Arino, GC Moore, JL Bustos… - … A European Journal, 2024 - Wiley Online Library
Spectator ions have known and emerging roles in aqueous metal‐cation chemistry,
respectively directing solubility, speciation, and reactivity. Here, we isolate and structurally …

Impact of Controlled Storage Conditions on the Hydrolysis and Surface Morphology of Amorphous-UO3

AB Hanson, IJ Schwerdt, CA Nizinski, RN Lee… - ACS …, 2021 - ACS Publications
The hydration and morphological effects of amorphous (A)-UO3 following storage under
varying temperature and relative humidity have been investigated. This study provides …

Pressure-induced structural and electronic phase transitions of uranium trioxide

JJ Ma, CB Zhang, R Qiu, P Zhang, B Ao, BT Wang - Physical Review B, 2021 - APS
The crystal structures, phonon spectra, and electronic properties of uranium trioxide (UO 3)
under high pressure have been systematically explored using a particle swarm optimization …

Model editing for distribution shifts in uranium oxide morphological analysis

D Brown, C Nizinski, M Shapiro… - Proceedings of the …, 2024 - openaccess.thecvf.com
Deep learning still struggles with certain kinds of scientific data. Notably pretraining data
may not provide coverage of relevant distribution shifts (eg shifts induced via the use of …

Effect of Diel Cycling Temperature, Relative Humidity, and Synthetic Route on the Surface Morphology and Hydrolysis of α-U3O8

AB Hanson, CA Nizinski, LW McDonald IV - ACS omega, 2021 - ACS Publications
The speciation and morphological changes of α-U3O8 following aging under diel cycling
temperature and relative humidity (RH) have been examined. This work advances the …

Ultrasonically assisted conversion of uranium trioxide into uranium (vi) intrinsic colloids

M Cot-Auriol, M Virot, C Micheau, T Dumas… - Dalton …, 2021 - pubs.rsc.org
Under oxidizing conditions, the corrosion of spent nuclear fuel may lead to the leaching of
radionuclides including soluble uranyl-based species. The speciation of the generated …

Trace Impurities Identified as Forensic Signatures in CMX-5 Fuel Pellets Using X-ray Spectroscopic Techniques

A van Veelen, SM Hickam, NP Edwards… - Analytical …, 2022 - ACS Publications
Small-particle analysis is a highly promising emerging forensic tool for analysis of interdicted
special nuclear materials. Integration of microstructural, morphological, compositional, and …

Structural Characterization of Uranium Tetrafluoride Hydrate (UF4·2.5H2O)

KJ Pastoor, AJ Miskowiec, JL Niedziela… - The Journal of …, 2022 - ACS Publications
Uranium tetrafluoride is an important intermediate in the nuclear fuel cycle. Facile synthesis
of its hydrate, uranium tetrafluoride hydrate (UF4· 2.5 H2O), has recently been reported. The …

Phase analysis of Australian uranium ore concentrates determined by variable temperature synchrotron powder x-ray diffraction

SB Pandelus, BJ Kennedy, G Murphy… - Inorganic …, 2021 - ACS Publications
The chemical speciation of uranium oxides is sensitive to the provenance of the samples
and their storage conditions. Here, we use diffraction methods to characterize the phases …