NMR for Single Ion Magnets

L Gigli, S Di Grande, E Ravera, G Parigi, C Luchinat - Magnetochemistry, 2021 - mdpi.com
Nuclear Magnetic Resonance is particularly sensitive to the electronic structure of matter
and is thus a powerful tool to characterize in-depth the magnetic properties of a system …

Observability of paramagnetic NMR signals at over 10 000 ppm chemical shifts

JC Ott, EA Suturina, I Kuprov, J Nehrkorn… - Angewandte …, 2021 - Wiley Online Library
We report an experimental observation of 31P NMR resonances shifted by over 10 000 ppm
(meaning percent range, and a new record for solutions), and similar 1H chemical shifts, in …

Modern physical methods for the molecular design of single-molecule magnets

VV Novikov, YV Nelyubina - Russian Chemical Reviews, 2021 - iopscience.iop.org
Many paramagnetic metal complexes have emerged as unique magnetic materials (single-
molecule magnets), which behave as conventional magnets at the single-molecule level …

Synthesis, X-ray structure and magnetic properties of the apically functionalized monocapped cobalt (ii) tris-pyridineoximates possessing SMM behaviour

AS Belov, SA Belova, NN Efimov, VV Zlobina… - Dalton …, 2023 - pubs.rsc.org
The title cobalt (II) pseudoclathrochelate complexes possess an intermediate trigonal
prismatic–trigonal antiprismatic geometry. As follows from PPMS data, they exhibit an SMM …

Selective Pathway toward Heteroleptic Spin-Crossover Iron(II) Complexes with Pyridine-Based N-Donor Ligands

I Nikovskiy, DY Aleshin, VV Novikov… - Inorganic …, 2022 - ACS Publications
A new synthetic pathway is devised to selectively produce previously elusive heteroleptic
iron (II) complexes of terpyridine and N, N′-disubstituted bis (pyrazol-3-yl) pyridines that …

Solvent-induced encapsulation of cobalt (II) ion by a boron-capped tris-pyrazoloximate

AS Belov, YZ Voloshin, AA Pavlov… - Inorganic …, 2020 - ACS Publications
Boron-cross-linked cobalt (II) pseudoclathrochelate was obtained by the template reaction of
2-acetylpyrazoloxime, phenylboronic acid, and a new DMF cobalt (II) solvato complex with a …

In Situ NMR Search for Spin-Crossover in Heteroleptic Cobalt(II) Complexes

Y Pankratova, D Aleshin, I Nikovskiy… - Inorganic …, 2020 - ACS Publications
Here we report the first successful attempt to identify spin-crossover compounds in solutions
of metal complexes produced by mixing different ligands and an appropriate metal salt by …

Towards the Molecular Design of Spin‐Crossover Complexes of 2, 6‐Bis (pyrazol‐3‐yl) pyridines

I Nikovskiy, A Polezhaev, V Novikov… - … A European Journal, 2020 - Wiley Online Library
The molecular design of spin‐crossover complexes relies on controlling the spin state of a
transition metal ion by proper chemical modifications of the ligands. Herein, the first N, N' …

Room-Temperature Spin Crossover in a Solution of Iron(II) Complexes with N,N′-Disubstituted Bis(pyrazol-3-yl)pyridines

DY Aleshin, I Nikovskiy, VV Novikov, AV Polezhaev… - ACS …, 2021 - ACS Publications
Here, we report a combined study of the effects of two chemical modifications to an N, N′-
disubstituted bis (pyrazol-3-yl) pyridine (3-bpp) and of different solvents on the spin …

A quantum chemistry view on two archetypical paramagnetic pentacoordinate nickel (II) complexes offers a fresh look on their NMR spectra

E Ravera, L Gigli, B Czarniecki, L Lang… - Inorganic …, 2021 - ACS Publications
Quantum chemical methods for calculating paramagnetic NMR observables are becoming
increasingly accessible and are being included in the inorganic chemistry practice. Here, we …