A field guide to flow chemistry for synthetic organic chemists

L Capaldo, Z Wen, T Noël - Chemical science, 2023 - pubs.rsc.org
Flow chemistry has unlocked a world of possibilities for the synthetic community, but the idea
that it is a mysterious “black box” needs to go. In this review, we show that several of the …

Technological innovations in photochemistry for organic synthesis: flow chemistry, high-throughput experimentation, scale-up, and photoelectrochemistry

L Buglioni, F Raymenants, A Slattery… - Chemical …, 2021 - ACS Publications
Photoinduced chemical transformations have received in recent years a tremendous amount
of attention, providing a plethora of opportunities to synthetic organic chemists. However …

Scale-up of photochemical reactions: transitioning from lab scale to industrial production

SDA Zondag, D Mazzarella… - Annual Review of …, 2023 - annualreviews.org
In the past two decades, we have witnessed a rapid emergence of new and powerful
photochemical and photocatalytic synthetic methods. Although these methods have been …

[HTML][HTML] Scale-up of micro-and milli-reactors: An overview of strategies, design principles and applications

Z Dong, Z Wen, F Zhao, S Kuhn, T Noël - Chemical Engineering Science: X, 2021 - Elsevier
Continuous-flow microreactor technology has been embraced by researchers in academia
and industry due to its excellent transport properties and the increased safety and control …

C(sp3)–H functionalizations of light hydrocarbons using decatungstate photocatalysis in flow

G Laudadio, Y Deng, K van der Wal, D Ravelli, M Nuño… - Science, 2020 - science.org
Direct activation of gaseous hydrocarbons remains a major challenge for the chemistry
community. Because of the intrinsic inertness of these compounds, harsh reaction conditions …

[HTML][HTML] Intensification strategies for improving the performance of photocatalytic processes: A review

DSM Constantino, MM Dias, AMT Silva, JL Faria… - Journal of Cleaner …, 2022 - Elsevier
Green and efficient technologies are one of the biggest challenges in Chemical
Engineering. Photocatalysis has been reported as one of the most promising eco-friendly …

Scalability of photochemical reactions in continuous flow mode

K Donnelly, M Baumann - Journal of Flow Chemistry, 2021 - Springer
Continuous flow photochemistry as a field has witnessed an increasing popularity over the
last decade in both academia and industry. Key drivers for this development are safety …

[HTML][HTML] Critical review on wastewater treatment using photo catalytic advanced oxidation process: Role of photocatalytic materials, reactor design and kinetics

J Iyyappan, B Gaddala, R Gnanasekaran… - Case Studies in …, 2024 - Elsevier
The presence of persistent organic compounds in wastewater poses significant challenges
to both biotic community and natural environment, resulting in a severely adverse effect on …

Multiphasic Continuous‐Flow Reactors for Handling Gaseous Reagents in Organic Synthesis: Enhancing Efficiency and Safety in Chemical Processes

AAH Laporte, TM Masson… - Angewandte Chemie …, 2024 - Wiley Online Library
The use of reactive gaseous reagents for the production of active pharmaceutical
ingredients (APIs) remains a scientific challenge due to safety and efficiency limitations. The …

Scale-up of a heterogeneous photocatalytic degradation using a photochemical rotor–stator spinning disk reactor

A Chaudhuri, SDA Zondag… - … Process Research & …, 2022 - ACS Publications
Many chemical reactions contain heterogeneous reagents, products, byproducts, or
catalysts, making their transposition from batch to continuous-flow processing challenging …