Dipolar recoupling under magic-angle spinning conditions

S Dusold, A Sebald - 2000 - Elsevier
Experimental NMR techniques designed to recouple weak homonuclear and heteronuclear
dipolar coupling interactions under magic-angle spinning conditions are discussed …

Atomic Resolution Structure of Monomorphic Aβ42 Amyloid Fibrils

MT Colvin, R Silvers, QZ Ni, TV Can… - Journal of the …, 2016 - ACS Publications
Amyloid-β (Aβ) is a 39–42 residue protein produced by the cleavage of the amyloid
precursor protein (APP), which subsequently aggregates to form cross-β amyloid fibrils that …

Map** of functional groups in metal-organic frameworks

X Kong, H Deng, F Yan, J Kim, JA Swisher, B Smit… - Science, 2013 - science.org
We determined the heterogeneous mesoscale spatial apportionment of functional groups in
a series of multivariate metal-organic frameworks (MTV-MOF-5) containing BDC (1, 4 …

Five decades of homonuclear dipolar decoupling in solid-state NMR: Status and outlook

KR Mote, V Agarwal, PK Madhu - Progress in nuclear magnetic resonance …, 2016 - Elsevier
It has been slightly more than fifty years since the first homonuclear spin decoupling
scheme, Lee-Goldburg decoupling, was proposed for removing homonuclear dipolar …

3D TEDOR NMR Experiments for the Simultaneous Measurement of Multiple Carbon−Nitrogen Distances in Uniformly 13C,15N-Labeled Solids

CP Jaroniec, C Filip, RG Griffin - Journal of the American …, 2002 - ACS Publications
We describe three-dimensional magic-angle-spinning NMR experiments for the
simultaneous measurement of multiple carbon− nitrogen distances in uniformly 13C, 15N …

Dephasing of spin echoes by multiple heteronuclear dipolar interactions in rotational echo double resonance NMR experiments

M Bertmer, H Eckert - Solid State Nuclear Magnetic Resonance, 1999 - Elsevier
The application of rotational echo double resonance (REDOR) nuclear magnetic resonance
(NMR) for accurate distance measurements has thus far been largely restricted to isolated …

Amphotericin B assembles into seven-molecule ion channels: An NMR and molecular dynamics study

Y Umegawa, T Yamamoto, M Dixit, K Funahashi… - Science …, 2022 - science.org
Amphotericin B, an antifungal drug with a long history of use, forms fungicidal ion-permeable
channels across cell membranes. Using solid-state nuclear magnetic resonance …

A solid-state NMR method for solution of zeolite crystal structures

DH Brouwer, RJ Darton, RE Morris… - Journal of the American …, 2005 - ACS Publications
Since zeolites are notoriously difficult to prepare as large single crystals, structure
determination usually relies on powder X-ray diffraction (XRD). However, structure solution …

Measurement of hetero-nuclear distances using a symmetry-based pulse sequence in solid-state NMR

L Chen, Q Wang, B Hu, O Lafon, J Trébosc… - Physical Chemistry …, 2010 - pubs.rsc.org
A Symmetry-based Resonance-Echo DOuble-Resonance (S-REDOR) method is proposed
for measuring hetero-nuclear dipolar couplings between two different spin-1/2 nuclei, under …

Three-dimensional structure determination of surface sites

P Berruyer, M Lelli, MP Conley… - Journal of the …, 2017 - ACS Publications
The spatial arrangement of atoms is directly linked to chemical function. A fundamental
challenge in surface chemistry and catalysis relates to the determination of three …