Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

[HTML][HTML] Solid-state NMR spectroscopy in pharmaceutical sciences

M Li, W Xu, Y Su - TrAC Trends in Analytical Chemistry, 2021 - Elsevier
Solid-state NMR (ssNMR) spectroscopy analyzes a wide range of pharmaceutical materials
in a non-disruptive and non-invasive manner. The obtained molecular properties at …

Protein data bank: a comprehensive review of 3D structure holdings and worldwide utilization by researchers, educators, and students

SK Burley, HM Berman, JM Duarte, Z Feng, JW Flatt… - Biomolecules, 2022 - mdpi.com
The Research Collaboratory for Structural Bioinformatics Protein Data Bank (RCSB PDB),
funded by the United States National Science Foundation, National Institutes of Health, and …

Identification and quantification of glycans in whole cells: architecture of microalgal polysaccharides described by solid-state nuclear magnetic resonance

A Poulhazan, MC Dickwella Widanage… - Journal of the …, 2021 - ACS Publications
Microalgae are photosynthetic organisms widely distributed in nature and serve as a
sustainable source of bioproducts. Their carbohydrate components are also promising …

From angstroms to nanometers: measuring interatomic distances by solid-state NMR

AA Shcherbakov, J Medeiros-Silva, N Tran… - Chemical …, 2021 - ACS Publications
Internuclear distances represent one of the main structural constraints in molecular structure
determination using solid-state NMR spectroscopy, complementing chemical shifts and …

Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems

L Liang, Y Ji, K Chen, P Gao, Z Zhao, G Hou - Chemical Reviews, 2022 - ACS Publications
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

Atomic-resolution chemical characterization of (2x)72-kDa tryptophan synthase via four- and five-dimensional 1H-detected solid-state NMR

A Klein, P Rovó, VV Sakhrani, Y Wang… - Proceedings of the …, 2022 - National Acad Sciences
NMR chemical shifts provide detailed information on the chemical properties of molecules,
thereby complementing structural data from techniques like X-ray crystallography and …

Early events in amyloid-β self-assembly probed by time-resolved solid state NMR and light scattering

J Jeon, WM Yau, R Tycko - Nature Communications, 2023 - nature.com
Self-assembly of amyloid-β peptides leads to oligomers, protofibrils, and fibrils that are likely
instigators of neurodegeneration in Alzheimer's disease. We report results of time-resolved …

Atomic-resolution structure of SARS-CoV-2 nucleocapsid protein N-terminal domain

S Sarkar, B Runge, RW Russell… - Journal of the …, 2022 - ACS Publications
The nucleocapsid (N) protein is one of the four structural proteins of the SARS-CoV-2 virus
and plays a crucial role in viral genome organization and, hence, replication and …