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Solid-state NMR of plant and fungal cell walls: a critical review
The cell walls of plants and microbes are a central source for bio-renewable energy and the
major targets of antibiotics and antifungal agents. It is highly challenging to determine the …
major targets of antibiotics and antifungal agents. It is highly challenging to determine the …
[HTML][HTML] Hidden motions and motion-induced invisibility: Dynamics-based spectral editing in solid-state NMR
Solid-state nuclear magnetic resonance (ssNMR) spectroscopy enables the structural
characterization of a diverse array of biological assemblies that include amyloid fibrils, non …
characterization of a diverse array of biological assemblies that include amyloid fibrils, non …
[PDF][PDF] Rapid natural-abundance 2D 13 C-13 C correlation spectroscopy using dynamic nuclear polarization enhanced solid-state NMR and matrix-free sample …
Solid-state nuclear magnetic resonance (SSNMR) has been extensively used to
characterize molecular structures at atomic scales.[1] Concerning biomolecular applications …
characterize molecular structures at atomic scales.[1] Concerning biomolecular applications …
Chemical shift computations on a crystallographic basis: some reflections and comments
Computations for chemical shifts of molecular organic compounds using the gauge‐
including projector augmented wave method and the NMR‐CASTEP code are reviewed …
including projector augmented wave method and the NMR‐CASTEP code are reviewed …
Proton to carbon-13 INEPT in solid-state NMR spectroscopy
A refocused INEPT through-bond coherence transfer technique is demonstrated for NMR of
rigid organic solids and is shown to provide a valuable building block for the development of …
rigid organic solids and is shown to provide a valuable building block for the development of …
Challenges and opportunities for alkane functionalisation using molecular catalysts
The conversion of vast low-value saturated hydrocarbons into valuable chemicals is of great
interest. Thanks to the progression of organometallic and coordination chemistry, transition …
interest. Thanks to the progression of organometallic and coordination chemistry, transition …
NMR Crystallography of Campho[2,3-c]pyrazole (Z′ = 6): Combining High-Resolution 1H-13C Solid-State MAS NMR Spectroscopy and GIPAW Chemical-Shift …
1H-13C two-dimensional magic-angle spinning (MAS) solid-state NMR correlation spectra,
recorded with the MAS-J-HMQC experiment, are presented for campho [2, 3-c] pyrazole. For …
recorded with the MAS-J-HMQC experiment, are presented for campho [2, 3-c] pyrazole. For …
Assigning carbon-13 NMR spectra to crystal structures by the INADEQUATE pulse sequence and first principles computation: a case study of two forms of testosterone
RK Harris, SA Joyce, CJ Pickard, S Cadars… - Physical Chemistry …, 2006 - pubs.rsc.org
A 13C CPMAS NMR experiment at high field (11.7 T) has produced significantly improved
dispersion for the α form of testosterone, allowing revisions and extensions to be made to …
dispersion for the α form of testosterone, allowing revisions and extensions to be made to …
Resolving structures from powders by NMR crystallography using combined proton spin diffusion and plane wave DFT calculations
We report a method that combines measured solid-state NMR chemical shifts and first
principles calculations to resolve the crystal structure of a powdered crystalline solid to …
principles calculations to resolve the crystal structure of a powdered crystalline solid to …
The refocused INADEQUATE MAS NMR experiment in multiple spin-systems: Interpreting observed correlation peaks and optimising lineshapes
The robustness of the refocused INADEQUATE MAS NMR pulse sequence for probing
through-bond connectivities has been demonstrated in a large range of solid-state …
through-bond connectivities has been demonstrated in a large range of solid-state …