Metrological characterization of X-ray diffraction methods for determination of crystallite size in nano-scale materials

V Uvarov, I Popov - Materials characterization, 2007 - Elsevier
Crystallite size values were determined by X-ray diffraction methods for 210 TiO2 (anatase)
nanocrystalline powders with crystallite size from 3 nm to 35 nm. Each X-ray diffraction …

Approximation of crystallite size and microstrain via XRD line broadening analysis in TiSiN thin films

AR Bushroa, RG Rahbari, HH Masjuki, MR Muhamad - Vacuum, 2012 - Elsevier
In the present work, an approximation method was used to determine both the crystallite size
and microstrain from XRD profile of TiSiN thin film deposited on high speed steel substrates …

Microstructure characterization of mechanically activated hematite using XRD line broadening

P Pourghahramani, E Forssberg - International Journal of Mineral …, 2006 - Elsevier
The effect of dry milling in a vibratory mill on the structural changes and microstructural
characteristics of hematite using different methods was investigated. We have described the …

Determination of structural elements of synthesized silver nano-hexagon from X-ray diffraction analysis

S Sarkar, R Das - 2018 - nopr.niscpr.res.in
Silver nano-hexagons (AgNHs) have been prepared by a chemical reduction method using
poly-vinyl pyrrolidone (PVP) as a stabilizing agent. The XRD results exhibit the crystalline …

Synthesis and characterization of W–Cu nanocomposites developed by mechanical alloying

SN Alam - Materials Science and Engineering: A, 2006 - Elsevier
In the present investigation, attempts have been made to synthesize W–Cu nanocomposites
by mechanical alloying (MA) and the results show that MA is a very good processing …

Efficient photodegradation of methylene blue (MB) under solar radiation by ZrC nanoparticles

AS Vig, A Gupta, OP Pandey - Advanced Powder Technology, 2018 - Elsevier
Due to increase in water pollution, there is a need to dwindle this problem for a clean and
green future. Photocatalysts like ZnO, CaO and TiO 2 have proved to be triumphant in …

[PDF][PDF] Program SizeCr for Calculation of the Microstructure parameters from X-ray Diffraction Data

AA Levin - Preprint, 2022 - researchgate.net
The SizeCr software package designed to input and calculate the parameters of the material
microstructure (crystallite size and microstrain in them) from the data of the XRD experiment …

[HTML][HTML] Titanium dioxide nanoparticles: synthesis, x-ray line analysis and chemical composition study

HM Chenari, C Seibel, D Hauschild, F Reinert… - Materials …, 2016 - SciELO Brasil
TiO2 nanoparticleshave been synthesized by the sol-gel method using titanium alkoxide
and isopropanolas a precursor. The structural properties and chemical composition of the …

Non-isothermal oxidation kinetics of nano-laminated Cr2AlC MAX phase

P Sharma, OP Pandey - Journal of Alloys and Compounds, 2019 - Elsevier
A highly pure Cr 2 AlC MAX phase is prepared through the sintering method by varying the
aluminum content. The non-isothermal oxidation kinetics of the Cr 2 AlC phase is examined …

Influence of carbon content of nano-TaC powders on the electrocatalytic and photocatalytic properties

LK Brar, A Gupta, OP Pandey - Catalysis Today, 2019 - Elsevier
Nano transition metal carbides (TMCs) have emerged as materials of great interest for
different catalytic applications in fuel cells and also as catalysts for photo-treatment of …