Hydrogen/deuterium exchange mass spectrometry for probing higher order structure of protein therapeutics: methodology and applications

H Wei, J Mo, L Tao, RJ Russell, AA Tymiak, G Chen… - Drug discovery today, 2014 - Elsevier
Highlights•Hydrogen/deuterium exchange mass spectrometry (HDX-MS) technology for
assessment of higher order structure of protein therapeutics.•Methodology: global HDX-MS …

Protein chemistry combined with mass spectrometry for protein structure determination

EV Petrotchenko, CH Borchers - Chemical Reviews, 2021 - ACS Publications
The advent of soft-ionization mass spectrometry for biomolecules has opened up new
possibilities for the structural analysis of proteins. Combining protein chemistry methods with …

Contemporary hydrogen deuterium exchange mass spectrometry

I Oganesyan, C Lento, DJ Wilson - Methods, 2018 - Elsevier
Hydrogen/deuterium exchange (HDX) mass spectrometry (MS) emerged as a tool for
biochemistry and structural biology around 25 years ago. It has since become a key …

Protein hydrogen exchange measured at single-residue resolution by electron transfer dissociation mass spectrometry

KD Rand, M Zehl, ON Jensen… - Analytical …, 2009 - ACS Publications
Because of unparalleled sensitivity and tolerance to protein size, mass spectrometry (MS)
has become a popular method for measuring the solution hydrogen (1H/2H) exchange (HX) …

Hydrogen/deuterium exchange mass spectrometry with top-down electron capture dissociation for characterizing structural transitions of a 17 kDa protein

J Pan, J Han, CH Borchers… - Journal of the American …, 2009 - ACS Publications
Amide H/D exchange (HDX) mass spectrometry (MS) is widely used for protein structural
studies. Traditionally, this technique involves protein labeling in D2O, followed by acid …

MSTools—Web based application for visualization and presentation of HXMS data

D Kavan, P Man - International journal of mass spectrometry, 2011 - Elsevier
Hydrogen/deuterium exchange coupled to mass spectrometry is an excellent technique to
study protein structure changes and interactions, especially in cases where traditional high …

Top-down mass spectrometry: recent developments, applications and perspectives

W Cui, HW Rohrs, ML Gross - Analyst, 2011 - pubs.rsc.org
Top-down mass spectrometry is an emerging approach for the analysis of intact proteins.
The term was coined as a contrast with the better-established, bottom-up strategy for …

Radical solutions: Principles and application of electron‐based dissociation in mass spectrometry‐based analysis of protein structure

F Lermyte, D Valkenborg, JA Loo… - Mass Spectrometry …, 2018 - Wiley Online Library
In recent years, electron capture (ECD) and electron transfer dissociation (ETD) have
emerged as two of the most useful methods in mass spectrometry‐based protein analysis …

Protein hydrogen exchange at residue resolution by proteolytic fragmentation mass spectrometry analysis

ZY Kan, BT Walters, L Mayne… - Proceedings of the …, 2013 - National Acad Sciences
Hydrogen exchange technology provides a uniquely powerful instrument for measuring
protein structural and biophysical properties, quantitatively and in a nonperturbing way, and …

Electron transfer dissociation facilitates the measurement of deuterium incorporation into selectively labeled peptides with single residue resolution

M Zehl, KD Rand, ON Jensen… - Journal of the American …, 2008 - ACS Publications
Mass spectrometry is routinely applied to measure the incorporation of deuterium into
proteins and peptides. The exchange of labile, heteroatom-bound hydrogens is mainly used …