Engineering of transition metal catalysts confined in zeolites

N Kosinov, C Liu, EJM Hensen, EA Pidko - Chemistry of Materials, 2018 - ACS Publications
Transition metal–zeolite composites are versatile catalytic materials for a wide range of
industrial and lab-scale processes. Significant advances in fabrication and characterization …

In situ and operando electron microscopy in heterogeneous catalysis—insights into multi-scale chemical dynamics

SW Chee, T Lunkenbein, R Schlögl… - Journal of Physics …, 2021 - iopscience.iop.org
This review features state-of-the-art in situ and operando electron microscopy (EM) studies
of heterogeneous catalysts in gas and liquid environments during reaction. Heterogeneous …

Three-dimensional quantification of the facet evolution of Pt nanoparticles in a variable gaseous environment

T Altantzis, I Lobato, A De Backer, A Béché, Y Zhang… - Nano …, 2018 - ACS Publications
Pt nanoparticles play an essential role in a wide variety of catalytic reactions. The activity of
the particles strongly depends on their three-dimensional (3D) structure and exposed facets …

Dynamic sparse x-ray nanotomography reveals ionomer hydration mechanism in polymer electrolyte fuel-cell catalyst

Z Gao, C Appel, M Holler, K Jeschonek… - Science …, 2024 - science.org
Tomographic imaging of time-evolving samples is a challenging yet important task for
various research fields. At the nanoscale, current approaches face limitations of …

Insights into chemical dynamics and their impact on the reactivity of Pt nanoparticles during CO oxidation by operando TEM

M Plodinec, HC Nerl, F Girgsdies, R Schlögl… - Acs …, 2020 - ACS Publications
The functionality of heterogeneous catalysts is influenced by a delicate interplay of multiple
parameters, including morphology and structure, chemical potential gradients and related …

Fast electron tomography for nanomaterials

W Albrecht, S Bals - The Journal of Physical Chemistry C, 2020 - ACS Publications
Electron tomography (ET) has become a well-established technique to visualize
nanomaterials in three dimensions. A vast richness in information can be gained by ET, but …

3D characterization of heat-induced morphological changes of Au nanostars by fast in situ electron tomography

H Vanrompay, E Bladt, W Albrecht, A Béché… - Nanoscale, 2018 - pubs.rsc.org
A thorough understanding of the thermal stability and potential resha** of anisotropic gold
nanostars is required for various potential applications. Combination of a tomographic …

Five-second STEM dislocation tomography for 300 nm thick specimen assisted by deep-learning-based noise filtering

Y Zhao, S Koike, R Nakama, S Ihara, M Mitsuhara… - Scientific reports, 2021 - nature.com
Scanning transmission electron microscopy (STEM) is suitable for visualizing the inside of a
relatively thick specimen than the conventional transmission electron microscopy, whose …

Fast electron tomography: Applications to beam sensitive samples and in situ TEM or operando environmental TEM studies

S Koneti, L Roiban, F Dalmas, C Langlois… - Materials …, 2019 - Elsevier
Electron Tomography (ET) is of greatest interest in studying nano-and biological materials
since it gives access to 3D morphological, chemical and physical features. Even though ET …

Fast versus conventional HAADF-STEM tomography of nanoparticles: advantages and challenges

H Vanrompay, A Skorikov, E Bladt, A Béché, B Freitag… - Ultramicroscopy, 2021 - Elsevier
HAADF-STEM tomography is a widely used experimental technique for analyzing
nanometer-scale structures of a large variety of materials in three dimensions. It is especially …