Aqueous microdroplets enable abiotic synthesis and chain extension of unique peptide isomers from free amino acids

DT Holden, NM Morato… - Proceedings of the …, 2022 - National Acad Sciences
Amide bond formation, the essential condensation reaction underlying peptide synthesis, is
hindered in aqueous systems by the thermodynamic constraints associated with …

Emerging microdroplet chemistry for synthesis and analysis

X Yan - International Journal of Mass Spectrometry, 2021 - Elsevier
Recent studies have shown that remarkable reaction acceleration can be achieved at the
air/solution interface of microdroplets. The unique environment of microdroplets can drive …

Chemical kinetics in microdroplets

KR Wilson, AM Prophet - Annual Review of Physical Chemistry, 2024 - annualreviews.org
Micrometer-sized compartments play significant roles in driving heterogeneous
transformations within atmospheric and biochemical systems as well as providing vehicles …

Electrostatics and chemical reactivity at the air–water interface

MTC Martins-Costa, MF Ruiz-López - Journal of the American …, 2023 - ACS Publications
It has been recently discovered that chemical reactions at aqueous interfaces can be orders
of magnitude faster compared to conventional bulk phase reactions, but despite its wide …

Accelerated reactions of amines with carbon dioxide driven by superacid at the microdroplet interface

KH Huang, Z Wei, RG Cooks - Chemical Science, 2021 - pubs.rsc.org
Microdroplets display distinctive interfacial chemistry, manifested as accelerated reactions
relative to those observed for the same reagents in bulk. Carbon dioxide undergoes C–N …

A critical analysis of electrospray techniques for the determination of accelerated rates and mechanisms of chemical reactions in droplets

G Rovelli, MI Jacobs, MD Willis, RJ Rapf… - Chemical …, 2020 - pubs.rsc.org
Electrospray and Electrosonic Spray Ionization Mass Spectrometry (ESI-MS and ESSI-MS)
have been widely used to report evidence that many chemical reactions in micro-and nano …

Water Charge Transfer Accelerates Criegee Intermediate Reaction with H2O Radical Anion at the Aqueous Interface

Q Liang, C Zhu, J Yang - Journal of the American Chemical …, 2023 - ACS Publications
Criegee intermediates (CIs) are important carbonyl oxides that may react with atmospheric
trace chemicals and impact the global climate. The CI reaction with water has been widely …

Aqueous microdroplets promote C–C bond formation and sequences in the reverse tricarboxylic acid cycle

Y Ju, H Zhang, Y Jiang, W Wang, G Kan, K Yu… - Nature Ecology & …, 2023 - nature.com
The reverse tricarboxylic acid cycle (rTCA) is a central anabolic network that uses carbon
dioxide (CO2) and may have provided complex carbon substrates for life before the advent …

A kinetic description of how interfaces accelerate reactions in micro-compartments

KR Wilson, AM Prophet, G Rovelli, MD Willis… - Chemical …, 2020 - pubs.rsc.org
A kinetic expression is derived to explain how interfaces alter bulk chemical equilibria and
accelerate reactions in micro-compartments. This description, aided by the development of a …

Accelerated microdroplet synthesis of benzimidazoles by nucleophilic addition to protonated carboxylic acids

P Basuri, LE Gonzalez, NM Morato, T Pradeep… - Chemical …, 2020 - pubs.rsc.org
We report a metal-free novel route for the accelerated synthesis of benzimidazole and its
derivatives in the ambient atmosphere. The synthetic procedure involves 1, 2-aromatic …