Solid-state NMR investigations of extracellular matrixes and cell walls of algae, bacteria, fungi, and plants

N Ghassemi, A Poulhazan, F Deligey… - Chemical …, 2021 - ACS Publications
Extracellular matrixes (ECMs), such as the cell walls and biofilms, are important for
supporting cell integrity and function and regulating intercellular communication. These …

[HTML][HTML] Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR

ASL Thankamony, JJ Wittmann, M Kaushik… - Progress in nuclear …, 2017 - Elsevier
The field of dynamic nuclear polarization has undergone tremendous developments and
diversification since its inception more than 6 decades ago. In this review we provide an in …

Dynamic nuclear polarization for sensitivity enhancement in biomolecular solid-state NMR

T Biedenbänder, V Aladin, S Saeidpour… - Chemical …, 2022 - ACS Publications
Solid-state NMR with magic-angle spinning (MAS) is an important method in structural
biology. While NMR can provide invaluable information about local geometry on an atomic …

[HTML][HTML] Solid-state NMR spectroscopy in pharmaceutical sciences

M Li, W Xu, Y Su - TrAC Trends in Analytical Chemistry, 2021 - Elsevier
Solid-state NMR (ssNMR) spectroscopy analyzes a wide range of pharmaceutical materials
in a non-disruptive and non-invasive manner. The obtained molecular properties at …

Recent developments in MAS DNP-NMR of materials

AGM Rankin, J Trébosc, F Pourpoint… - Solid State Nuclear …, 2019 - Elsevier
Solid-state NMR spectroscopy is a powerful technique for the characterization of the atomic-
level structure and dynamics of materials. Nevertheless, the use of this technique is often …

Dynamic nuclear polarization enhancement of 200 at 21.15 T enabled by 65 kHz magic angle spinning

P Berruyer, S Björgvinsdóttir… - The journal of …, 2020 - ACS Publications
Solid-state nuclear magnetic resonance under magic angle spinning (MAS) enhanced with
dynamic nuclear polarization (DNP) is a powerful approach to characterize many important …

Highly efficient polarizing agents for MAS‐DNP of proton‐dense molecular solids

R Harrabi, T Halbritter, F Aussenac… - Angewandte …, 2022 - Wiley Online Library
Efficiently hyperpolarizing proton‐dense molecular solids through dynamic nuclear
polarization (DNP) solid‐state NMR is still an unmet challenge. Polarizing agents (PAs) …

TinyPols: a family of water-soluble binitroxides tailored for dynamic nuclear polarization enhanced NMR spectroscopy at 18.8 and 21.1 T

A Lund, G Casano, G Menzildjian, M Kaushik… - Chemical …, 2020 - pubs.rsc.org
Dynamic Nuclear Polarization (DNP) has recently emerged as a key method to increase the
sensitivity of solid-state NMR spectroscopy under Magic Angle Spinning (MAS). While …

Computationally assisted design of polarizing agents for dynamic nuclear polarization enhanced NMR: the AsymPol family

F Mentink-Vigier, I Marin-Montesinos… - Journal of the …, 2018 - ACS Publications
We introduce a new family of highly efficient polarizing agents for dynamic nuclear
polarization (DNP)-enhanced nuclear magnetic resonance (NMR) applications, composed …

BDPA-nitroxide biradicals tailored for efficient dynamic nuclear polarization enhanced solid-state NMR at magnetic fields up to 21.1 T

D Wisser, G Karthikeyan, A Lund… - Journal of the …, 2018 - ACS Publications
Dynamic nuclear polarization (DNP) solid-state nuclear magnetic resonance (NMR) has
developed into an invaluable tool for the investigation of a wide range of materials …