Solid‐state NMR spectroscopic methods in chemistry

DD Laws, HML Bitter, A Jerschow - Angewandte Chemie …, 2002 - Wiley Online Library
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …

Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems

L Liang, Y Ji, K Chen, P Gao, Z Zhao, G Hou - Chemical reviews, 2022 - ACS Publications
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

3D TEDOR NMR Experiments for the Simultaneous Measurement of Multiple Carbon−Nitrogen Distances in Uniformly 13C,15N-Labeled Solids

CP Jaroniec, C Filip, RG Griffin - Journal of the American …, 2002 - ACS Publications
We describe three-dimensional magic-angle-spinning NMR experiments for the
simultaneous measurement of multiple carbon− nitrogen distances in uniformly 13C, 15N …

Fast magic-angle sample spinning solid-state NMR at 60–100 kHz for natural abundance samples

Y Nishiyama - Solid State Nuclear Magnetic Resonance, 2016 - Elsevier
In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

Acid properties of solid acid catalysts characterized by solid-state 31P NMR of adsorbed phosphorous probe molecules

A Zheng, SJ Huang, SB Liu, F Deng - Physical Chemistry Chemical …, 2011 - pubs.rsc.org
A brief review is presented on acidity characterization of solid acid catalysts by means of
solid-state phosphor-31 magic-angle-spinning nuclear magnetic resonance (31P MAS …

Dipolar Recoupling in Rotating Solids

V Ladizhansky, RS Palani, M Mardini… - Chemical …, 2024 - ACS Publications
Magic angle spinning (MAS) nuclear magnetic resonance (NMR) has evolved significantly
over the past three decades and established itself as a vital tool for the structural analysis of …

Structural constraints from proton-mediated rare-spin correlation spectroscopy in rotating solids

A Lange, S Luca, M Baldus - Journal of the American Chemical …, 2002 - ACS Publications
A novel solid-state NMR concept is introduced that allows for the detection of through-space
proton− proton contacts in high spectral resolution. The proposed method not only can be …

Symmetry principles in the nuclear magnetic resonance of spinning solids: heteronuclear recoupling by generalized Hartmann–Hahn sequences

A Brinkmann, MH Levitt - The Journal of chemical physics, 2001 - pubs.aip.org
General symmetry principles for rotor-synchronized pulse sequences in magic-angle
spinning solid-state nuclear magnetic resonance are presented. The theory of symmetry …

Floquet theory in solid-state nuclear magnetic resonance

M Leskes, PK Madhu, S Vega - Progress in nuclear magnetic resonance …, 2010 - Elsevier
Nuclear magnetic resonance (NMR) spectroscopy deals with time-dependent perturbations
of nuclear spin systems and it is often imperative to solve the time-dependent Schrödinger …

Solid-state NMR study of the transformation of octacalcium phosphate to hydroxyapatite: a mechanistic model for central dark line formation

YH Tseng, CY Mou, JCC Chan - Journal of the American …, 2006 - ACS Publications
For many years, octacalcium phosphate (OCP) has been postulated as the precursor phase
of biological apatite in bones and teeth. In this work, we study the molecular mechanism of …