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Insight into the structures and dynamics of organic semiconductors through solid-state NMR spectroscopy
Organic semiconductors (OSCs) are of fundamental and technological interest, owing to
their properties and functions in a range of optoelectronic devices, including organic light …
their properties and functions in a range of optoelectronic devices, including organic light …
Dipolar recoupling in magic angle spinning solid-state nuclear magnetic resonance
G De Paëpe - Annual review of physical chemistry, 2012 - annualreviews.org
Solid-state nuclear magnetic resonance (SSNMR) magic angle spinning (MAS) can be used
to record high-resolution data dominated by site-specific information. Although MAS …
to record high-resolution data dominated by site-specific information. Although MAS …
Proton assisted recoupling and protein structure determination
We introduce a homonuclear version of third spin assisted recoupling, a second-order
mechanism that can be used for polarization transfer between C 13 or N 15 spins in magic …
mechanism that can be used for polarization transfer between C 13 or N 15 spins in magic …
Direct spectral optimisation of proton–proton homonuclear dipolar decoupling in solid-state NMR
We show how direct spectral optimisation can be used to provide significantly improved
resolution for proton NMR spectroscopy in the solid state. We describe the design of new …
resolution for proton NMR spectroscopy in the solid state. We describe the design of new …
[HTML][HTML] 1H line width dependence on MAS speed in solid state NMR–Comparison of experiment and simulation
Recent developments in magic angle spinning (MAS) technology permit spinning
frequencies of≥ 100 kHz. We examine the effect of such fast MAS rates upon nuclear …
frequencies of≥ 100 kHz. We examine the effect of such fast MAS rates upon nuclear …
Origins of linewidth in H1 magic-angle spinning NMR
VE Zorin, SP Brown, P Hodgkinson - The Journal of chemical physics, 2006 - pubs.aip.org
A detailed study of the factors determining the linewidth (and hence resolution) in H 1 solid-
state magic-angle spinning NMR is described. Although it has been known from the early …
state magic-angle spinning NMR is described. Although it has been known from the early …
Backbone Assignment of Fully Protonated Solid Proteins by 1H Detection and Ultrafast Magic‐Angle‐Spinning NMR Spectroscopy
A Marchetti, S Jehle, M Felletti… - Angewandte Chemie …, 2012 - Wiley Online Library
In the past decade solid-state magic-angle-spinning (MAS) NMR spectroscopy has emerged
as a unique technique for obtaining information on the atomic-level structure and dynamics …
as a unique technique for obtaining information on the atomic-level structure and dynamics …
Dipolar recoupling in fast-MAS solid-state NMR spectroscopy
I Schnell - Progress in Nuclear Magnetic Resonance …, 2004 - Elsevier
In view of the success of high-resolution NMR [1–6], in particular recalling the Nobel prizes
awarded to Ernst [7] and Wüthrich [8], one might be tempted to say that solid-state NMR …
awarded to Ernst [7] and Wüthrich [8], one might be tempted to say that solid-state NMR …
Assigning carbon-13 NMR spectra to crystal structures by the INADEQUATE pulse sequence and first principles computation: a case study of two forms of testosterone
RK Harris, SA Joyce, CJ Pickard, S Cadars… - Physical Chemistry …, 2006 - pubs.rsc.org
A 13C CPMAS NMR experiment at high field (11.7 T) has produced significantly improved
dispersion for the α form of testosterone, allowing revisions and extensions to be made to …
dispersion for the α form of testosterone, allowing revisions and extensions to be made to …
Proton-detected solid-state NMR reveals intramembrane polar networks in a seven-helical transmembrane protein proteorhodopsin
We used high-resolution proton-detected multidimensional NMR to study the solvent-
exposed parts of a seven-helical integral membrane proton pump, proteorhodopsin (PR) …
exposed parts of a seven-helical integral membrane proton pump, proteorhodopsin (PR) …