Insight into the structures and dynamics of organic semiconductors through solid-state NMR spectroscopy

M Seifrid, GNM Reddy, BF Chmelka… - Nature Reviews …, 2020 - nature.com
Organic semiconductors (OSCs) are of fundamental and technological interest, owing to
their properties and functions in a range of optoelectronic devices, including organic light …

Dipolar recoupling in magic angle spinning solid-state nuclear magnetic resonance

G De Paëpe - Annual review of physical chemistry, 2012 - annualreviews.org
Solid-state nuclear magnetic resonance (SSNMR) magic angle spinning (MAS) can be used
to record high-resolution data dominated by site-specific information. Although MAS …

Proton assisted recoupling and protein structure determination

G De Paëpe, JR Lewandowski, A Loquet… - The Journal of …, 2008 - pubs.aip.org
We introduce a homonuclear version of third spin assisted recoupling, a second-order
mechanism that can be used for polarization transfer between C 13 or N 15 spins in magic …

Direct spectral optimisation of proton–proton homonuclear dipolar decoupling in solid-state NMR

B Elena, G de Paëpe, L Emsley - Chemical physics letters, 2004 - Elsevier
We show how direct spectral optimisation can be used to provide significantly improved
resolution for proton NMR spectroscopy in the solid state. We describe the design of new …

[HTML][HTML] 1H line width dependence on MAS speed in solid state NMR–Comparison of experiment and simulation

U Sternberg, R Witter, I Kuprov, JM Lamley… - Journal of Magnetic …, 2018 - Elsevier
Recent developments in magic angle spinning (MAS) technology permit spinning
frequencies of≥ 100 kHz. We examine the effect of such fast MAS rates upon nuclear …

Origins of linewidth in H1 magic-angle spinning NMR

VE Zorin, SP Brown, P Hodgkinson - The Journal of chemical physics, 2006 - pubs.aip.org
A detailed study of the factors determining the linewidth (and hence resolution) in H 1 solid-
state magic-angle spinning NMR is described. Although it has been known from the early …

Backbone Assignment of Fully Protonated Solid Proteins by 1H Detection and Ultrafast Magic‐Angle‐Spinning NMR Spectroscopy

A Marchetti, S Jehle, M Felletti… - Angewandte Chemie …, 2012 - Wiley Online Library
In the past decade solid-state magic-angle-spinning (MAS) NMR spectroscopy has emerged
as a unique technique for obtaining information on the atomic-level structure and dynamics …

Dipolar recoupling in fast-MAS solid-state NMR spectroscopy

I Schnell - Progress in Nuclear Magnetic Resonance …, 2004 - Elsevier
In view of the success of high-resolution NMR [1–6], in particular recalling the Nobel prizes
awarded to Ernst [7] and Wüthrich [8], one might be tempted to say that solid-state NMR …

Assigning carbon-13 NMR spectra to crystal structures by the INADEQUATE pulse sequence and first principles computation: a case study of two forms of testosterone

RK Harris, SA Joyce, CJ Pickard, S Cadars… - Physical Chemistry …, 2006 - pubs.rsc.org
A 13C CPMAS NMR experiment at high field (11.7 T) has produced significantly improved
dispersion for the α form of testosterone, allowing revisions and extensions to be made to …

Proton-detected solid-state NMR reveals intramembrane polar networks in a seven-helical transmembrane protein proteorhodopsin

ME Ward, L Shi, E Lake, S Krishnamurthy… - Journal of the …, 2011 - ACS Publications
We used high-resolution proton-detected multidimensional NMR to study the solvent-
exposed parts of a seven-helical integral membrane proton pump, proteorhodopsin (PR) …