Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

NMR studies of organic polymorphs & solvates

RK Harris - Analyst, 2006 - pubs.rsc.org
This review article describes the applications of NMR to the study of polymorphs and related
forms (solvates) of organic (especially pharmaceutical) compounds, for which it is of …

The use of NMR spectroscopy to study tautomerism

RM Claramunt, C López, MD Santa María… - Progress in Nuclear …, 2006 - Elsevier
This review is a summary of the enormous literature describing applications of NMR
spectroscopy to tautomerism. Almost all the publications dealing with tautomerism, since the …

Insights into biomolecular hydrogen bonds from hydrogen bond scalar couplings

S Grzesiek, F Cordier, V Jaravine, M Barfield - Progress in Nuclear …, 2004 - Elsevier
Despite their crucial role in the stabilization of biomolecular structures and their almost
ubiquitous involvement in biomolecular reactions, such as enzymatic cleavage or ligand …

Solid-state NMR spectroscopy for the analysis of element-based non-covalent interactions

Y Xu, PMJ Szell, V Kumar, DL Bryce - Coordination Chemistry Reviews, 2020 - Elsevier
We review applications of solid-state NMR spectroscopy for the analysis of element-based
non-covalent interactions, with an emphasis on developments since 2009. The review is …

15N NMR spectroscopy in structural analysis: an update (2001-2005)

R Marek, A Lycka, E Kolehmainen… - Current Organic …, 2007 - ingentaconnect.com
Since our previous review article (Curr. Org. Chem. 2002, 6, 35), significant improvements
and an array of 15N NMR applications in structural analysis have been published. This …

Imidazole–imidazole hydrogen bonding in the pH-sensing histidine side chains of influenza A M2

KT Movellan, M Wegstroth, K Overkamp… - Journal of the …, 2020 - ACS Publications
The arrangement of histidine side chains in influenza A M2 tetramer determines their p K a
values, which define pH-controlled proton conduction critical to the virus lifecycle. Both water …

NMR response of the tetrel bond donor

SA Southern, T Nag, V Kumar, M Triglav… - The Journal of …, 2021 - ACS Publications
The tetrel elements (group 14) have the capacity to act as electrophilic sites and participate
in structure-directing noncovalent tetrel bonds. We establish here the experimental response …

The refocused INADEQUATE MAS NMR experiment in multiple spin-systems: Interpreting observed correlation peaks and optimising lineshapes

S Cadars, J Sein, L Duma, A Lesage, TN Pham… - Journal of Magnetic …, 2007 - Elsevier
The robustness of the refocused INADEQUATE MAS NMR pulse sequence for probing
through-bond connectivities has been demonstrated in a large range of solid-state …

Recent advances in solid-state NMR spectroscopy of spin I= 1/2 nuclei

A Lesage - Physical Chemistry Chemical Physics, 2009 - pubs.rsc.org
This perspective contains a brief review of some of the most recent developments in solid-
state NMR spectroscopy of spin I= 1/2 nuclei. Over the last few years, methodological …