Experimental designs and their recent advances in set-up, data interpretation, and analytical applications

B Dejaegher, Y Vander Heyden - Journal of pharmaceutical and …, 2011 - Elsevier
In this review, the set-up and data interpretation of experimental designs (screening,
response surface, and mixture designs) are discussed. Advanced set-ups considered are …

Ruggedness and robustness testing

B Dejaegher, Y Vander Heyden - Journal of chromatography A, 2007 - Elsevier
Due to the strict regulatory requirements, especially in pharmaceutical analysis, analysis
results with an acceptable quality should be reported. Thus, a proper validation of the …

Induced sample via transient isotachophoresis mediated with swee** in micellar electrokinetic chromatography for the dual-stacking strategy of non-steroidal anti …

NF Semail, ASA Keyon, B Saad… - … of Chromatography A, 2022 - Elsevier
Realising the need to devise a simple, sensitive, and reliable detection method, this study
investigated the development of a dual-stacking transient isotachophoresis (t-ITP) and …

Capillary electrophoresis for the analysis of small‐molecule pharmaceuticals

K Altria, A Marsh, C Sänger‐van de Griend - Electrophoresis, 2006 - Wiley Online Library
This paper reviews the application of CE to the analysis of small‐molecule pharmaceuticals.
The areas of pharmaceutical analysis covered are enantiomer separation, the analysis of …

Response surface optimization for determination of pesticide multiresidues by matrix solid-phase dispersion and gas chromatography

YY Hu, P Zheng, YZ He, GP Sheng - Journal of Chromatography A, 2005 - Elsevier
An optimized multiresidue analysis method based on matrix solid-phase dispersion (MSPD)
and gas chromatography (GC) is proposed for the determination of organochlorines and …

Quality by Design approach in the development of a solvent-modified micellar electrokinetic chromatography method: Finding the design space for the determination …

S Furlanetto, S Orlandini, B Pasquini, M Del Bubba… - Analytica Chimica …, 2013 - Elsevier
A solvent-modified micellar electrokinetic chromatography method was set up for the
simultaneous determination of the tricyclic antidepressant amitriptyline (AMI) and its main …

An integrated quality by design and mixture-process variable approach in the development of a capillary electrophoresis method for the analysis of almotriptan and its …

S Orlandini, B Pasquini, M Stocchero, S Pinzauti… - … of Chromatography A, 2014 - Elsevier
The development of a capillary electrophoresis (CE) method for the assay of almotriptan
(ALM) and its main impurities using an integrated Quality by Design and mixture-process …

Electrokinetic supercharging for on-line preconcentration of seven non-steroidal anti-inflammatory drugs in water samples

M Dawod, MC Breadmore, RM Guijt… - … of Chromatography A, 2008 - Elsevier
The development of new sensitive methods for the analysis of non-steroidal anti-
inflammatory drugs (NSAIDs) in water samples is of great importance. In this work, seven …

Development and validation of a high-performance thin-layer chromatographic method for the simultaneous determination of two binary mixtures containing ketorolac …

FA El Yazbi, EM Hassan, EF Khamis… - Journal of …, 2016 - academic.oup.com
A validated and highly selective high-performance thin-layer chromatography (HPTLC)
method was developed for the determination of ketorolac tromethamine (KTC) with …

Recent advances in micellar electrokinetic chromatography

TJ Pappas, M Gayton‐Ely, LA Holland - Electrophoresis, 2005 - Wiley Online Library
This review contains nearly 200 reference citations, and covers advances in electrokinetic
capillary chromatography based on micelles, including stabilized micelle complexes …