Experimental designs and their recent advances in set-up, data interpretation, and analytical applications
B Dejaegher, Y Vander Heyden - Journal of pharmaceutical and …, 2011 - Elsevier
In this review, the set-up and data interpretation of experimental designs (screening,
response surface, and mixture designs) are discussed. Advanced set-ups considered are …
response surface, and mixture designs) are discussed. Advanced set-ups considered are …
Ruggedness and robustness testing
B Dejaegher, Y Vander Heyden - Journal of chromatography A, 2007 - Elsevier
Due to the strict regulatory requirements, especially in pharmaceutical analysis, analysis
results with an acceptable quality should be reported. Thus, a proper validation of the …
results with an acceptable quality should be reported. Thus, a proper validation of the …
Induced sample via transient isotachophoresis mediated with swee** in micellar electrokinetic chromatography for the dual-stacking strategy of non-steroidal anti …
Realising the need to devise a simple, sensitive, and reliable detection method, this study
investigated the development of a dual-stacking transient isotachophoresis (t-ITP) and …
investigated the development of a dual-stacking transient isotachophoresis (t-ITP) and …
Capillary electrophoresis for the analysis of small‐molecule pharmaceuticals
K Altria, A Marsh, C Sänger‐van de Griend - Electrophoresis, 2006 - Wiley Online Library
This paper reviews the application of CE to the analysis of small‐molecule pharmaceuticals.
The areas of pharmaceutical analysis covered are enantiomer separation, the analysis of …
The areas of pharmaceutical analysis covered are enantiomer separation, the analysis of …
Response surface optimization for determination of pesticide multiresidues by matrix solid-phase dispersion and gas chromatography
YY Hu, P Zheng, YZ He, GP Sheng - Journal of Chromatography A, 2005 - Elsevier
An optimized multiresidue analysis method based on matrix solid-phase dispersion (MSPD)
and gas chromatography (GC) is proposed for the determination of organochlorines and …
and gas chromatography (GC) is proposed for the determination of organochlorines and …
Quality by Design approach in the development of a solvent-modified micellar electrokinetic chromatography method: Finding the design space for the determination …
A solvent-modified micellar electrokinetic chromatography method was set up for the
simultaneous determination of the tricyclic antidepressant amitriptyline (AMI) and its main …
simultaneous determination of the tricyclic antidepressant amitriptyline (AMI) and its main …
An integrated quality by design and mixture-process variable approach in the development of a capillary electrophoresis method for the analysis of almotriptan and its …
The development of a capillary electrophoresis (CE) method for the assay of almotriptan
(ALM) and its main impurities using an integrated Quality by Design and mixture-process …
(ALM) and its main impurities using an integrated Quality by Design and mixture-process …
Electrokinetic supercharging for on-line preconcentration of seven non-steroidal anti-inflammatory drugs in water samples
The development of new sensitive methods for the analysis of non-steroidal anti-
inflammatory drugs (NSAIDs) in water samples is of great importance. In this work, seven …
inflammatory drugs (NSAIDs) in water samples is of great importance. In this work, seven …
Development and validation of a high-performance thin-layer chromatographic method for the simultaneous determination of two binary mixtures containing ketorolac …
A validated and highly selective high-performance thin-layer chromatography (HPTLC)
method was developed for the determination of ketorolac tromethamine (KTC) with …
method was developed for the determination of ketorolac tromethamine (KTC) with …
Recent advances in micellar electrokinetic chromatography
This review contains nearly 200 reference citations, and covers advances in electrokinetic
capillary chromatography based on micelles, including stabilized micelle complexes …
capillary chromatography based on micelles, including stabilized micelle complexes …