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Dynamic nuclear polarization for sensitivity enhancement in biomolecular solid-state NMR
Solid-state NMR with magic-angle spinning (MAS) is an important method in structural
biology. While NMR can provide invaluable information about local geometry on an atomic …
biology. While NMR can provide invaluable information about local geometry on an atomic …
[HTML][HTML] Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR
ASL Thankamony, JJ Wittmann, M Kaushik… - Progress in nuclear …, 2017 - Elsevier
The field of dynamic nuclear polarization has undergone tremendous developments and
diversification since its inception more than 6 decades ago. In this review we provide an in …
diversification since its inception more than 6 decades ago. In this review we provide an in …
Biomolecular and biological applications of solid-state NMR with dynamic nuclear polarization enhancement
Solid-state NMR spectroscopy (ssNMR) with magic-angle spinning (MAS) enables the
investigation of biological systems within their native context, such as lipid membranes, viral …
investigation of biological systems within their native context, such as lipid membranes, viral …
Highly efficient, water‐soluble polarizing agents for dynamic nuclear polarization at high frequency
C Sauvée, M Rosay, G Casano… - Angewandte Chemie …, 2013 - Wiley Online Library
Dynamic nuclear polarization coupled to solid-state NMR spectroscopy (DNP/ssNMR) is
emerging as a very powerful technique to overcome the limitations resulting from the …
emerging as a very powerful technique to overcome the limitations resulting from the …
Facing and overcoming sensitivity challenges in biomolecular NMR spectroscopy
In the Spring of 2013, NMR spectroscopists convened at the Weizmann Institute in Israel to
brainstorm on approaches to improve the sensitivity of NMR experiments, particularly when …
brainstorm on approaches to improve the sensitivity of NMR experiments, particularly when …
Large molecular weight nitroxide biradicals providing efficient dynamic nuclear polarization at temperatures up to 200 K
A Zagdoun, G Casano, O Ouari… - Journal of the …, 2013 - ACS Publications
A series of seven functionalized nitroxide biradicals (the bTbK biradical and six derivatives)
are investigated as exogenous polarization sources for dynamic nuclear polarization (DNP) …
are investigated as exogenous polarization sources for dynamic nuclear polarization (DNP) …
Rational design of dinitroxide biradicals for efficient cross-effect dynamic nuclear polarization
DJ Kubicki, G Casano, M Schwarzwälder, S Abel… - Chemical …, 2016 - pubs.rsc.org
A series of 37 dinitroxide biradicals have been prepared and their performance studied as
polarizing agents in cross-effect DNP NMR experiments at 9.4 T and 100 K in 1, 1, 2, 2 …
polarizing agents in cross-effect DNP NMR experiments at 9.4 T and 100 K in 1, 1, 2, 2 …
Magic Angle Spinning NMR of Proteins: High-Frequency Dynamic Nuclear Polarization and 1H Detection
Magic angle spinning (MAS) NMR studies of amyloid and membrane proteins and large
macromolecular complexes are an important new approach to structural biology. However …
macromolecular complexes are an important new approach to structural biology. However …
DNP NMR of biomolecular assemblies
Abstract Dynamic Nuclear Polarization (DNP) is an effective approach to alleviate the
inherently low sensitivity of solid-state NMR (ssNMR) under magic angle spinning (MAS) …
inherently low sensitivity of solid-state NMR (ssNMR) under magic angle spinning (MAS) …
Targeted DNP for biomolecular solid-state NMR
High-field dynamic nuclear polarization is revolutionizing the scope of solid-state NMR with
new applications in surface chemistry, materials science and structural biology. In this …
new applications in surface chemistry, materials science and structural biology. In this …