In Situ and Emerging Transmission Electron Microscopy for Catalysis Research

HY Chao, K Venkatraman, S Moniri, Y Jiang… - Chemical …, 2023 - ACS Publications
Catalysts are the primary facilitator in many dynamic processes. Therefore, a thorough
understanding of these processes has vast implications for a myriad of energy systems. The …

Single-crystal structure determination of nanosized metal–organic frameworks by three-dimensional electron diffraction

T Yang, T Willhammar, H Xu, X Zou, Z Huang - Nature Protocols, 2022 - nature.com
Metal–organic frameworks (MOFs) have attracted considerable interest due to their well-
defined pore architecture and structural tunability on molecular dimensions. While single …

Jana2020 – a new version of the crystallographic computing system Jana

V Petříček, L Palatinus, J Plášil… - Zeitschrift für …, 2023 - degruyter.com
We present the crystallographic program Jana2020, the successor of Jana2006. Jana2020
has new, technically different graphics and structure plot-driven intuitive control. Tools …

Accurate structure models and absolute configuration determination using dynamical effects in continuous-rotation 3D electron diffraction data

PB Klar, Y Krysiak, H Xu, G Steciuk, J Cho, X Zou… - Nature Chemistry, 2023 - nature.com
Continuous-rotation 3D electron diffraction methods are increasingly popular for the
structure analysis of very small organic molecular crystals and crystalline inorganic …

Atomic-level structure determination of amorphous molecular solids by NMR

M Cordova, P Moutzouri, SO Nilsson Lill… - Nature …, 2023 - nature.com
Abstract Structure determination of amorphous materials remains challenging, owing to the
disorder inherent to these materials. Nuclear magnetic resonance (NMR) powder …

A 3D extra-large-pore zeolite enabled by 1D-to-3D topotactic condensation of a chain silicate

J Li, ZR Gao, QF Lin, C Liu, F Gao, C Lin, S Zhang… - Science, 2023 - science.org
Zeolites are microporous silicates with a large variety of applications as catalysts,
adsorbents, and cation exchangers. Stable silica-based zeolites with increased porosity are …

Single entity electrocatalysis

TB Clarke, LE Krushinski, KJ Vannoy… - Chemical …, 2024 - ACS Publications
Making a measurement over millions of nanoparticles or exposed crystal facets seldom
reports on reactivity of a single nanoparticle or facet, which may depart drastically from …

3D electron diffraction for chemical analysis: Instrumentation developments and innovative applications

T Gruene, E Mugnaioli - Chemical Reviews, 2021 - ACS Publications
In the past few years, many exciting papers reported results based on crystal structure
determination by electron diffraction. The aim of this review is to provide general and …

MyD88 TIR domain higher-order assembly interactions revealed by microcrystal electron diffraction and serial femtosecond crystallography

MTB Clabbers, S Holmes, TW Muusse… - Nature …, 2021 - nature.com
MyD88 and MAL are Toll-like receptor (TLR) adaptors that signal to induce pro-inflammatory
cytokine production. We previously observed that the TIR domain of MAL (MALTIR) forms …

Hydrogen atoms in supramolecular chemistry: a structural perspective. Where are they, and why does it matter?

AL Thompson, NG White - Chemical Society Reviews, 2023 - pubs.rsc.org
Hydrogen bonding interactions are ubiquitous across the biochemical and chemical
sciences, and are of particular interest to supramolecular chemists. They have been used to …